About: Synthesis of esters derived from 2,3,4,6-tetra-O-acetyl-1-[4-(2-hydroxyethyl)-1H-1,2,3-triazol-1-yl]-beta-D-glucopyranose

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About: Synthesis of esters derived from 2,3,4,6-tetra-O-acetyl-1-[4-(2-hydroxyethyl)-1H-1,2,3-triazol-1-yl]-beta-D-glucopyranose Goto Sponge NotDistinct Permalink

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	2,3,4,6-Tetra-O-acetyl-1-[4-(2-hydroxyethyl)- 1H-1,2,3-triazol-1-yl]-beta-D-glucopyranose was prepared and reacted with several acids, either commercially available or prepared. These included, aliphatic or aromatic acids (phenylacetic acid derivatives, benzoic derivatives), palmitic acid and the protected amino acids N-(benzyloxycarbonyl)glycine and N-(tert- butyloxycarbonyl)phenylalanine. Two other acids, 2-(3-bromopropoxy)benzoic acid and 2- (5-bromopentoxy)benzoic acid (analogues of salicylic acid were synthesized), whose preparation is also described in this work. The esterification was performed either with N,N'- dicyclohexylcarbodiimide (DCC)/4-dimethylaminopyridine (DMAP) or by reacting the acyl chlorides with the alcohol in the presence of triethylamine. The products were isolated in fair yields and fully characterized by the usual analytical techniques. 2,3,4,6-Tetra-O-acetyl-1-[4-(2-hydroxyethyl)- 1H-1,2,3-triazol-1-yl]-beta-D-glucopyranose was prepared and reacted with several acids, either commercially available or prepared. These included, aliphatic or aromatic acids (phenylacetic acid derivatives, benzoic derivatives), palmitic acid and the protected amino acids N-(benzyloxycarbonyl)glycine and N-(tert- butyloxycarbonyl)phenylalanine. Two other acids, 2-(3-bromopropoxy)benzoic acid and 2- (5-bromopentoxy)benzoic acid (analogues of salicylic acid were synthesized), whose preparation is also described in this work. The esterification was performed either with N,N'- dicyclohexylcarbodiimide (DCC)/4-dimethylaminopyridine (DMAP) or by reacting the acyl chlorides with the alcohol in the presence of triethylamine. The products were isolated in fair yields and fully characterized by the usual analytical techniques. (en)
Title	Synthesis of esters derived from 2,3,4,6-tetra-O-acetyl-1-[4-(2-hydroxyethyl)-1H-1,2,3-triazol-1-yl]-beta-D-glucopyranose Synthesis of esters derived from 2,3,4,6-tetra-O-acetyl-1-[4-(2-hydroxyethyl)-1H-1,2,3-triazol-1-yl]-beta-D-glucopyranose (en)
skos:prefLabel	Synthesis of esters derived from 2,3,4,6-tetra-O-acetyl-1-[4-(2-hydroxyethyl)-1H-1,2,3-triazol-1-yl]-beta-D-glucopyranose Synthesis of esters derived from 2,3,4,6-tetra-O-acetyl-1-[4-(2-hydroxyethyl)-1H-1,2,3-triazol-1-yl]-beta-D-glucopyranose (en)
skos:notation	RIV/00216275:25310/13:39896179!RIV14-MSM-25310___
http://linked.open...avai/predkladatel	Fakulta chemicko-technologická
http://linked.open...avai/riv/aktivita	I
http://linked.open...avai/riv/aktivity	I
http://linked.open...iv/cisloPeriodika	1
http://linked.open...vai/riv/dodaniDat	2014
http://linked.open...aciTvurceVysledku	Hrdina, Radim Marques Dinis Pinto, Tiago Alexandre
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Univerzita Pardubice / Fakulta chemicko-technologická
http://linked.open...dnocenehoVysledku	109530
http://linked.open...ai/riv/idVysledku	RIV/00216275:25310/13:39896179
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	Phenyl acetic acid derivatives; Benzoic acid derivatives; Click chemistry Glycoconjugates; 1,2,3-Triazoles Glucopyranose (en)
http://linked.open.../riv/klicoveSlovo	3-Triazoles Glucopyranose Benzoic acid derivatives Click chemistry Glycoconjugates Phenyl acetic acid derivatives 1 2
http://linked.open...odStatuVydavatele	US - Spojené státy americké
http://linked.open...ontrolniKodProRIV	[0FDDA8EFBF5F]
http://linked.open...i/riv/nazevZdroje	European Journal of Chemistry
http://linked.open...in/vavai/riv/obor	CC
http://linked.open...ichTvurcuVysledku	2 (xsd:int)
http://linked.open...cetTvurcuVysledku	7 (xsd:int)
http://linked.open...UplatneniVysledku	2013
http://linked.open...v/svazekPeriodika	4
http://linked.open...iv/tvurceVysledku	Hrdina, Radim Cunha, Silvia Esteves, Ana Marques Dinis Pinto, Tiago Alexandre Oliveira-Campos, Ana Rodrigues, Ligia Silva, Marillia
issn	2153-2249
number of pages	6 (xsd:int)
http://bibframe.org/vocab/doi	10.5155/eurjchem.4.1.64-69.735
http://localhost/t...ganizacniJednotka	25310

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