About: Use of S-Mosher acid as a chiral solvating agent for enantiomeric analysis of some trans-4-(4-fluorophenyl)-3-substituted-1-methylpiperidines by means of NMR spectroscopy     Goto   Sponge   NotDistinct   Permalink

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Description
  • S-Mosher acid induced chemical-shift non-equivalence in NMR spectra of chiral trans-4-(4-fluorophenyl)-3-substituted-1-methylpiperidines. The magnitude of Dd in 1H and 19F NMR spectra varied with the substituent at position 3 of the piperidine ring. The magnitudes Dd observed for certain protons and for the fluorine in the 4-fluorophenyl group were sufficiently large to allow determination of enantiomeric composition.
  • S-Mosher acid induced chemical-shift non-equivalence in NMR spectra of chiral trans-4-(4-fluorophenyl)-3-substituted-1-methylpiperidines. The magnitude of Dd in 1H and 19F NMR spectra varied with the substituent at position 3 of the piperidine ring. The magnitudes Dd observed for certain protons and for the fluorine in the 4-fluorophenyl group were sufficiently large to allow determination of enantiomeric composition. (en)
Title
  • Use of S-Mosher acid as a chiral solvating agent for enantiomeric analysis of some trans-4-(4-fluorophenyl)-3-substituted-1-methylpiperidines by means of NMR spectroscopy
  • Use of S-Mosher acid as a chiral solvating agent for enantiomeric analysis of some trans-4-(4-fluorophenyl)-3-substituted-1-methylpiperidines by means of NMR spectroscopy (en)
skos:prefLabel
  • Use of S-Mosher acid as a chiral solvating agent for enantiomeric analysis of some trans-4-(4-fluorophenyl)-3-substituted-1-methylpiperidines by means of NMR spectroscopy
  • Use of S-Mosher acid as a chiral solvating agent for enantiomeric analysis of some trans-4-(4-fluorophenyl)-3-substituted-1-methylpiperidines by means of NMR spectroscopy (en)
skos:notation
  • RIV/00216224:14330/01:00005424!RIV/2002/MSM/143302/N
http://linked.open.../vavai/riv/strany
  • 731
http://linked.open...avai/riv/aktivita
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  • Z(MSM 143100011)
http://linked.open...iv/cisloPeriodika
  • 10
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
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  • 699784
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  • RIV/00216224:14330/01:00005424
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  • spectral non-equivalence; piperidines; NMR; paroxetine (en)
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  • CZ - Česká republika
http://linked.open...ontrolniKodProRIV
  • [995947A607C1]
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  • Chirality
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http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 13
http://linked.open...iv/tvurceVysledku
  • Navrátilová, Hana
http://linked.open...n/vavai/riv/zamer
issn
  • 0899-0042
number of pages
http://localhost/t...ganizacniJednotka
  • 14330
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