About: The Reaction of [P3N3Cl4(NH2)2] with [HN(POCl2)2]; the Crystal Structure of a Phosphazenium Salt [P3N3HCl4(NH2)2]+ [N(POCl2)2]-.

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About: The Reaction of [P3N3Cl4(NH2)2] with [HN(POCl2)2]; the Crystal Structure of a Phosphazenium Salt [P3N3HCl4(NH2)2]+ [N(POCl2)2]-. Goto Sponge NotDistinct Permalink

An Entity of Type : http://linked.opendata.cz/ontology/domain/vavai/Vysledek, within Data Space : linked.opendata.cz associated with source document(s)

Attributes	Values
rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	Reakcí P3N3Cl4(NH2)2 s HCl v acetonitrilu lze připravit ve vysokém výtěžku P3N3Cl5(NH2), jehož krystalová struktura byla určena RTG strukturní analýzou. Při použití diethyletheru nebo dichlormethanu vzniká při této reakci fosfazeniová sůl [P3N3Cl4H(NH2)2]+Cl-. Diskutována byla vibrační spektra obou látek a studováno jejich termické chování. (cs) P3N3Cl5(NH2) in high purity and good yield can be obtained by the reaction of P3N3Cl4(NH2)2 with gaseous HCl in acetonitrile If diethylether or dichlormethane is used as a solvent, a salt-like compound [P3N3Cl4H(NH2)2+Cl- is formed as a microcrystalline product instead of P3N3Cl5(NH2). The crystal structure of P3N3Cl5(NH2)was determined by X-ray structure analysis. Vibrational spectra and thermic behavior of both P3N3Cl5(NH2)and [P3N3Cl4H(NH2)2+Cl- are also briefly discussed. P3N3Cl5(NH2) in high purity and good yield can be obtained by the reaction of P3N3Cl4(NH2)2 with gaseous HCl in acetonitrile If diethylether or dichlormethane is used as a solvent, a salt-like compound [P3N3Cl4H(NH2)2+Cl- is formed as a microcrystalline product instead of P3N3Cl5(NH2). The crystal structure of P3N3Cl5(NH2)was determined by X-ray structure analysis. Vibrational spectra and thermic behavior of both P3N3Cl5(NH2)and [P3N3Cl4H(NH2)2+Cl- are also briefly discussed. (en)
Title	Reakce P3N3Cl4(NH2)2 s HCl: krystalová struktura P3N3Cl5(NH2). (cs) The Reaction of [P3N3Cl4(NH2)2] with [HN(POCl2)2]; the Crystal Structure of a Phosphazenium Salt [P3N3HCl4(NH2)2]+ [N(POCl2)2]-. The Reaction of [P3N3Cl4(NH2)2] with [HN(POCl2)2]; the Crystal Structure of a Phosphazenium Salt [P3N3HCl4(NH2)2]+ [N(POCl2)2]-. (en)
skos:prefLabel	Reakce P3N3Cl4(NH2)2 s HCl: krystalová struktura P3N3Cl5(NH2). (cs) The Reaction of [P3N3Cl4(NH2)2] with [HN(POCl2)2]; the Crystal Structure of a Phosphazenium Salt [P3N3HCl4(NH2)2]+ [N(POCl2)2]-. The Reaction of [P3N3Cl4(NH2)2] with [HN(POCl2)2]; the Crystal Structure of a Phosphazenium Salt [P3N3HCl4(NH2)2]+ [N(POCl2)2]-. (en)
skos:notation	RIV/00216224:14310/97:00003795!RIV08-GA0-14310___
http://linked.open.../vavai/riv/strany	637
http://linked.open...avai/riv/aktivita	P
http://linked.open...avai/riv/aktivity	P(GA203/95/1190)
http://linked.open...iv/cisloPeriodika	623
http://linked.open...vai/riv/dodaniDat	2008
http://linked.open...aciTvurceVysledku	Alberti, Milan Marek, Jaromír Břínek, Josef Toužín, Jiří
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Masarykova univerzita / Přírodovědecká fakulta
http://linked.open...dnocenehoVysledku	811015
http://linked.open...ai/riv/idVysledku	RIV/00216224:14310/97:00003795
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	preparation; crystal structure; molecular structure; vibrational spectra (en)
http://linked.open.../riv/klicoveSlovo	vibrational spectra molecular structure crystal structure preparation
http://linked.open...odStatuVydavatele	DE - Spolková republika Německo
http://linked.open...ontrolniKodProRIV	[31A4B66A226D]
http://linked.open...i/riv/nazevZdroje	Zeitschrift für anorganische und allgemeine Chemie [Bd. 380 (1971) -]
http://linked.open...in/vavai/riv/obor	CA
http://linked.open...ichTvurcuVysledku	4 (xsd:int)
http://linked.open...cetTvurcuVysledku	4 (xsd:int)
http://linked.open...vavai/riv/projekt	Structure and Bonding in the Compounds of Nitrogen,Phosphorus,Sulfur and Selenium and in the Complexes of Fe,Co,and Ni with N,P,S-Ligands
http://linked.open...UplatneniVysledku	1997
http://linked.open...v/svazekPeriodika	1997
http://linked.open...iv/tvurceVysledku	Alberti, Milan Marek, Jaromír Břínek, Josef Toužín, Jiří
issn	0044-2313
number of pages	5 (xsd:int)
http://localhost/t...ganizacniJednotka	14310

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