About: Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	Development of LC/MS/MS method for analysing polycyclic aromatic nitrogen hydrocarbons (PANHs) in soil samples is presented. Optimisation of individual chromatographic/mass spectrometric conditions was made in order to obtain a method for the determination of 15 PANHs content in an organic extract from the soil. Detection limits (LOD) in the range of 0.3 to 15 pg per injection were 15 obtained for individual PANHs. LC/MS/MS method has a lower LOD value compared to LC/DAD/FLD methods in general. Developed LC/MS/MS method was used for determination of PANHs content in soil samples collected in contaminated areas of the southeast region of the Czech Republic. Highest concentrations of PANHs have been found in the samples collected in the immediate vicinity of the industrial basin. Concentrations of the contaminants in samples collected in surrounding villages were higher compared to the sample collected in clean area of the Czech Republic. Development of LC/MS/MS method for analysing polycyclic aromatic nitrogen hydrocarbons (PANHs) in soil samples is presented. Optimisation of individual chromatographic/mass spectrometric conditions was made in order to obtain a method for the determination of 15 PANHs content in an organic extract from the soil. Detection limits (LOD) in the range of 0.3 to 15 pg per injection were 15 obtained for individual PANHs. LC/MS/MS method has a lower LOD value compared to LC/DAD/FLD methods in general. Developed LC/MS/MS method was used for determination of PANHs content in soil samples collected in contaminated areas of the southeast region of the Czech Republic. Highest concentrations of PANHs have been found in the samples collected in the immediate vicinity of the industrial basin. Concentrations of the contaminants in samples collected in surrounding villages were higher compared to the sample collected in clean area of the Czech Republic. (en)
Title	Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry (en)
skos:prefLabel	Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry (en)
skos:notation	RIV/00216224:14310/09:00036101!RIV10-MSM-14310___
http://linked.open...avai/riv/aktivita	S Z
http://linked.open...avai/riv/aktivity	S, Z(MSM0021622412)
http://linked.open...iv/cisloPeriodika	No. 3
http://linked.open...vai/riv/dodaniDat	2010
http://linked.open...aciTvurceVysledku	Švábenský, Radim Oravec, Michal Šimek, Zdeněk
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Masarykova univerzita / Přírodovědecká fakulta
http://linked.open...dnocenehoVysledku	309928
http://linked.open...ai/riv/idVysledku	RIV/00216224:14310/09:00036101
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	polycyclic aromatic nitrogen heterocycles; PANHs; soil; LC-ESI/MS/MS (en)
http://linked.open.../riv/klicoveSlovo	LC-ESI/MS/MS PANHs polycyclic aromatic nitrogen heterocycles soil
http://linked.open...odStatuVydavatele	GB - Spojené království Velké Británie a Severního Irska
http://linked.open...ontrolniKodProRIV	[F1633067171C]
http://linked.open...i/riv/nazevZdroje	International Journal of Environmental analytical cemistry
http://linked.open...in/vavai/riv/obor	CB
http://linked.open...ichTvurcuVysledku	3 (xsd:int)
http://linked.open...cetTvurcuVysledku	3 (xsd:int)
http://linked.open...UplatneniVysledku	2009
http://linked.open...v/svazekPeriodika	Vol. 89
http://linked.open...iv/tvurceVysledku	Šimek, Zdeněk Oravec, Michal Švábenský, Radim
http://linked.open...n/vavai/riv/zamer	Interactions among the chemicals, environment and biological systems and their consequences on the global, regional and local scales (INCHEMBIOL)
issn	0306-7319
number of pages	15 (xsd:int)
http://localhost/t...ganizacniJednotka	14310
is http://linked.open...avai/riv/vysledek of	Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry

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