About: Reactions of P4S10 and pyPS2Cl with N,N-diphenylurea and N,N-diphenylthiourea     Goto   Sponge   NotDistinct   Permalink

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  • The reaction of P4S10 (1) with N,N-diphenylurea (PhNH)2CO (2) results in new heterocyclic compounds containing the (PSN)2 cycle and the cyclic thiophosphates [pyH]2[P2S8] (5), [pyH]2[P2S7] (6) and [pyH]3[P3S9] (7). A similar reaction, but carried out with N,N -diphenylthiourea (PhNH)2CS (8), leads to the formation of 4 and 6. pyPS2Cl (9), used as an alternative starting material, also yields compounds 3, 4, 5, and further [pyH][PS2Cl2] (10) and S8 after reaction with 2. Compound 3 reacts with Pd(CH3COO)2, with the formation of the complex [Pd(Ph2N2COPS2)2] (11). The crystal structures of 3 and 7 were determined by single crystal X-ray diffraction.
  • The reaction of P4S10 (1) with N,N-diphenylurea (PhNH)2CO (2) results in new heterocyclic compounds containing the (PSN)2 cycle and the cyclic thiophosphates [pyH]2[P2S8] (5), [pyH]2[P2S7] (6) and [pyH]3[P3S9] (7). A similar reaction, but carried out with N,N -diphenylthiourea (PhNH)2CS (8), leads to the formation of 4 and 6. pyPS2Cl (9), used as an alternative starting material, also yields compounds 3, 4, 5, and further [pyH][PS2Cl2] (10) and S8 after reaction with 2. Compound 3 reacts with Pd(CH3COO)2, with the formation of the complex [Pd(Ph2N2COPS2)2] (11). The crystal structures of 3 and 7 were determined by single crystal X-ray diffraction. (en)
Title
  • Reactions of P4S10 and pyPS2Cl with N,N-diphenylurea and N,N-diphenylthiourea
  • Reactions of P4S10 and pyPS2Cl with N,N-diphenylurea and N,N-diphenylthiourea (en)
skos:prefLabel
  • Reactions of P4S10 and pyPS2Cl with N,N-diphenylurea and N,N-diphenylthiourea
  • Reactions of P4S10 and pyPS2Cl with N,N-diphenylurea and N,N-diphenylthiourea (en)
skos:notation
  • RIV/00216224:14310/07:00032323!RIV10-MSM-14310___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • S
http://linked.open...iv/cisloPeriodika
  • 26
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 446488
http://linked.open...ai/riv/idVysledku
  • RIV/00216224:14310/07:00032323
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • Chlorodithiophosphoric acid pyridiniumbetaine; Phosphorus pentasulfide; Diazaphosphetidine; Cyclic thiophosphates; Palladium(II) complex (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • CZ - Česká republika
http://linked.open...ontrolniKodProRIV
  • [2C85E216E31A]
http://linked.open...i/riv/nazevZdroje
  • Polyhedron
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 2007
http://linked.open...iv/tvurceVysledku
  • Nečas, Marek
  • Dastych, Dalibor
  • Dastychová, Lenka
  • Příhoda, Jiří
  • Sotolářová, Marie
  • Taraba, Jan
http://linked.open...ain/vavai/riv/wos
  • 000249905900028
issn
  • 0277-5387
number of pages
http://localhost/t...ganizacniJednotka
  • 14310
is http://linked.open...avai/riv/vysledek of
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