About: Examination of sol-gel technique applicability for preparation of pellets for soil analysis by laser ablation inductively coupled plasma optical emission spectrometry     Goto   Sponge   NotDistinct   Permalink

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  • Silica sol - gel matter was examined as a binder assisting the preparation of agricultural soil sample pellets for elemental analysis by laser ablation inductively coupled plasma optical emission spectrometry. The sol - gel method, allowing homogenous dispersion of internal standard ( Sc) and analytes in calibration pellets, was applied to the determination of Cr, Ni, Cu, Zn and Pb in four types of soils. A Q-switched Nd:YAG laser ( 1064 nm) was employed for ablation of pellets prepared by pressing of a ground and homogenized blend of soil and silica gel. Calibration curves exhibited correlation coefficients greater than 0.997. The repeatability of determination for elements of interest did not exceed 7% RSD. Accuracy of determination was proved by X-ray. fluorescence analysis.
  • Silica sol - gel matter was examined as a binder assisting the preparation of agricultural soil sample pellets for elemental analysis by laser ablation inductively coupled plasma optical emission spectrometry. The sol - gel method, allowing homogenous dispersion of internal standard ( Sc) and analytes in calibration pellets, was applied to the determination of Cr, Ni, Cu, Zn and Pb in four types of soils. A Q-switched Nd:YAG laser ( 1064 nm) was employed for ablation of pellets prepared by pressing of a ground and homogenized blend of soil and silica gel. Calibration curves exhibited correlation coefficients greater than 0.997. The repeatability of determination for elements of interest did not exceed 7% RSD. Accuracy of determination was proved by X-ray. fluorescence analysis. (en)
Title
  • Examination of sol-gel technique applicability for preparation of pellets for soil analysis by laser ablation inductively coupled plasma optical emission spectrometry
  • Examination of sol-gel technique applicability for preparation of pellets for soil analysis by laser ablation inductively coupled plasma optical emission spectrometry (en)
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  • Examination of sol-gel technique applicability for preparation of pellets for soil analysis by laser ablation inductively coupled plasma optical emission spectrometry
  • Examination of sol-gel technique applicability for preparation of pellets for soil analysis by laser ablation inductively coupled plasma optical emission spectrometry (en)
skos:notation
  • RIV/00216224:14310/07:00023742!RIV10-MSM-14310___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(MSM0021622412)
http://linked.open...iv/cisloPeriodika
  • 10
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 421000
http://linked.open...ai/riv/idVysledku
  • RIV/00216224:14310/07:00023742
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • laser ablation; sol-gel; inductively coupled plasma; optical emission spectrometry; soil (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • GB - Spojené království Velké Británie a Severního Irska
http://linked.open...ontrolniKodProRIV
  • [74CFC55C88D1]
http://linked.open...i/riv/nazevZdroje
  • JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 22/2007
http://linked.open...iv/tvurceVysledku
  • Kanický, Viktor
  • Pinkas, Jiří
  • Holá, Markéta
  • Janotková, Ivona
http://linked.open...ain/vavai/riv/wos
  • 000249925600011
http://linked.open...n/vavai/riv/zamer
issn
  • 0267-9477
number of pages
http://localhost/t...ganizacniJednotka
  • 14310
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