About: UV and IR laser ablation study of natural organic powdered materials—an example: ICP-OES with laser ablation of spiked infant formula cast pellets     Goto   Sponge   NotDistinct   Permalink

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Description
  • Laser ablation (LA) sample introduction into inductively coupled plasma optical emission spectrometry (ICP-OES) was used for powdered infant food formula being representative of samples with an organic matrix. Milk samples enriched with eight naturally occurring elements were presented for LA-ICP-OES experiments as cast epoxy resin disks. For Ca, Cu, Fe, Mg and Zn, a performance of IR (1064 nm) and UV (266 nm) ablation was compared in a fixed spot mode (UV) and in a scanning mode (both UV and IR). Signal vs. content dependences proved to be linear both with and w/o the internal standard Ca (IS). Using the IS the linear regression parameters for the scanning mode were improved for both UV and IR ablation. The UV fixed spot ablation provided the closest correlation and so, except for Cu (low content), repeatability for all elements of interest did not exceed 10% RSD. Lowest determinable quantities were 0.06% Ca, 0.008% Mg, 0.0005% Cu, 0.001% Fe and 0.0008% Zn.
  • Laser ablation (LA) sample introduction into inductively coupled plasma optical emission spectrometry (ICP-OES) was used for powdered infant food formula being representative of samples with an organic matrix. Milk samples enriched with eight naturally occurring elements were presented for LA-ICP-OES experiments as cast epoxy resin disks. For Ca, Cu, Fe, Mg and Zn, a performance of IR (1064 nm) and UV (266 nm) ablation was compared in a fixed spot mode (UV) and in a scanning mode (both UV and IR). Signal vs. content dependences proved to be linear both with and w/o the internal standard Ca (IS). Using the IS the linear regression parameters for the scanning mode were improved for both UV and IR ablation. The UV fixed spot ablation provided the closest correlation and so, except for Cu (low content), repeatability for all elements of interest did not exceed 10% RSD. Lowest determinable quantities were 0.06% Ca, 0.008% Mg, 0.0005% Cu, 0.001% Fe and 0.0008% Zn. (en)
Title
  • UV and IR laser ablation study of natural organic powdered materials—an example: ICP-OES with laser ablation of spiked infant formula cast pellets
  • UV and IR laser ablation study of natural organic powdered materials—an example: ICP-OES with laser ablation of spiked infant formula cast pellets (en)
skos:prefLabel
  • UV and IR laser ablation study of natural organic powdered materials—an example: ICP-OES with laser ablation of spiked infant formula cast pellets
  • UV and IR laser ablation study of natural organic powdered materials—an example: ICP-OES with laser ablation of spiked infant formula cast pellets (en)
skos:notation
  • RIV/00216224:14310/06:00018199!RIV10-MSM-14310___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(MSM0021622411), Z(MSM0021622412)
http://linked.open...iv/cisloPeriodika
  • 9
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 505509
http://linked.open...ai/riv/idVysledku
  • RIV/00216224:14310/06:00018199
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • laser ablation; powder; infant formula; inductively coupled plasma; atomic emission spectrometry (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • GB - Spojené království Velké Británie a Severního Irska
http://linked.open...ontrolniKodProRIV
  • [2871CD84B5CC]
http://linked.open...i/riv/nazevZdroje
  • Journal of analytical atomic spectrometry
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 21/2006
http://linked.open...iv/tvurceVysledku
  • Kanický, Viktor
  • Otruba, Vítězslav
  • Holá, Markéta
  • Krásenský, Pavel
http://linked.open...ain/vavai/riv/wos
  • 000240082600018
http://linked.open...n/vavai/riv/zamer
issn
  • 0267-9477
number of pages
http://localhost/t...ganizacniJednotka
  • 14310
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