About: On the reactions of chlorodithiophosphoric acid pyridiniumbetaine with polyfunctional nucleophiles. Part III: Reactions with monoalkylderivatives of thiosemicarbazide     Goto   Sponge   NotDistinct   Permalink

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  • Reactions of chlorodithiophosphoric acid pyridinium betaine, py.PS2Cl, (I) with monosubstituted thiosemicarbazide derivatives RN(H)C(S)N(H)NH2, (R = methyl, ethyl), in acetonitrile media and in the presence of pyridine as an HCl acceptor were studied. New five-membered heterocyclic compounds were prepared, pyridinium salts of 4-methyl-3-sulfido-3,5-dithioxo-1,2,4,3-triazaphospholidine (II) and 4-ethyl-3-sulfido-3,5-dithioxo-1,2,4,3-triazaphospholidine (III). The substances II and III were completely characterized by 31P NMR, FT-IR, Raman spectroscopies and their molecular structures were determined by the X-ray diffraction analysis.
  • Reactions of chlorodithiophosphoric acid pyridinium betaine, py.PS2Cl, (I) with monosubstituted thiosemicarbazide derivatives RN(H)C(S)N(H)NH2, (R = methyl, ethyl), in acetonitrile media and in the presence of pyridine as an HCl acceptor were studied. New five-membered heterocyclic compounds were prepared, pyridinium salts of 4-methyl-3-sulfido-3,5-dithioxo-1,2,4,3-triazaphospholidine (II) and 4-ethyl-3-sulfido-3,5-dithioxo-1,2,4,3-triazaphospholidine (III). The substances II and III were completely characterized by 31P NMR, FT-IR, Raman spectroscopies and their molecular structures were determined by the X-ray diffraction analysis. (en)
Title
  • On the reactions of chlorodithiophosphoric acid pyridiniumbetaine with polyfunctional nucleophiles. Part III: Reactions with monoalkylderivatives of thiosemicarbazide
  • On the reactions of chlorodithiophosphoric acid pyridiniumbetaine with polyfunctional nucleophiles. Part III: Reactions with monoalkylderivatives of thiosemicarbazide (en)
skos:prefLabel
  • On the reactions of chlorodithiophosphoric acid pyridiniumbetaine with polyfunctional nucleophiles. Part III: Reactions with monoalkylderivatives of thiosemicarbazide
  • On the reactions of chlorodithiophosphoric acid pyridiniumbetaine with polyfunctional nucleophiles. Part III: Reactions with monoalkylderivatives of thiosemicarbazide (en)
skos:notation
  • RIV/00216224:14310/05:00013951!RIV10-MSM-14310___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(MSM 143100011)
http://linked.open...iv/cisloPeriodika
  • 14
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 534507
http://linked.open...ai/riv/idVysledku
  • RIV/00216224:14310/05:00013951
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • Five-membered heterocycle; thiosemicarbazide; chlorodithiophosphoric acid pyridinium betaine (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • CZ - Česká republika
http://linked.open...ontrolniKodProRIV
  • [DEC35CB05589]
http://linked.open...i/riv/nazevZdroje
  • Polyhedron
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 24
http://linked.open...iv/tvurceVysledku
  • Nečas, Marek
  • Příhoda, Jiří
  • Ševčík, Richard
http://linked.open...n/vavai/riv/zamer
issn
  • 0277-5387
number of pages
http://localhost/t...ganizacniJednotka
  • 14310
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