About: Isolation of Quaternary Benzo[c] phenanthridine Alkaloids from Macleaya microcarpa (MAXIM.) FEDDE: Comparison of Maceration, Soxhlet Extraction and Pressurised Liquid Extraction

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	Macleaya microcarpa (Papaveraceae family) has been of considerable interest in recent years as a prospective source of quaternary benzo[c]phenanthridine alkaloids (QBAs) related to many pharmaceutical beneficial effects. For this purpose, a quantitative, efficient and fast method to isolate the QBAs from the plant material is required. To optimise and compare pressurised liquid extraction (PLE) with Soxhlet extraction and maceration in order to estimate extraction conditions for fast and efficient isolation of QBAs contained in the roots of Macleaya microcarpa. The QBAs were extracted by PLE, Soxhlet extraction and maceration at different conditions (solvent, time, etc.). Reversed phase HPLC with diode-array detector was utilised for their determination and quantification. To optimise the PLE procedure, the variable parameters, including temperature (40C-150C), sample-to-inert material ratio, extraction time (5-30 min) and number of extraction cycles (1-4), were also tested. Macleaya microcarpa (Papaveraceae family) has been of considerable interest in recent years as a prospective source of quaternary benzo[c]phenanthridine alkaloids (QBAs) related to many pharmaceutical beneficial effects. For this purpose, a quantitative, efficient and fast method to isolate the QBAs from the plant material is required. To optimise and compare pressurised liquid extraction (PLE) with Soxhlet extraction and maceration in order to estimate extraction conditions for fast and efficient isolation of QBAs contained in the roots of Macleaya microcarpa. The QBAs were extracted by PLE, Soxhlet extraction and maceration at different conditions (solvent, time, etc.). Reversed phase HPLC with diode-array detector was utilised for their determination and quantification. To optimise the PLE procedure, the variable parameters, including temperature (40C-150C), sample-to-inert material ratio, extraction time (5-30 min) and number of extraction cycles (1-4), were also tested. (en)
Title	Isolation of Quaternary Benzo[c] phenanthridine Alkaloids from Macleaya microcarpa (MAXIM.) FEDDE: Comparison of Maceration, Soxhlet Extraction and Pressurised Liquid Extraction Isolation of Quaternary Benzo[c] phenanthridine Alkaloids from Macleaya microcarpa (MAXIM.) FEDDE: Comparison of Maceration, Soxhlet Extraction and Pressurised Liquid Extraction (en)
skos:prefLabel	Isolation of Quaternary Benzo[c] phenanthridine Alkaloids from Macleaya microcarpa (MAXIM.) FEDDE: Comparison of Maceration, Soxhlet Extraction and Pressurised Liquid Extraction Isolation of Quaternary Benzo[c] phenanthridine Alkaloids from Macleaya microcarpa (MAXIM.) FEDDE: Comparison of Maceration, Soxhlet Extraction and Pressurised Liquid Extraction (en)
skos:notation	RIV/00216224:14110/12:00057370!RIV13-GA0-14110___
http://linked.open...avai/predkladatel	Lékařská fakulta
http://linked.open...avai/riv/aktivita	P S Z
http://linked.open...avai/riv/aktivity	P(GA525/08/0819), P(GAP206/11/0138), P(GPP503/11/P523), S, Z(AV0Z40310501)
http://linked.open...iv/cisloPeriodika	5
http://linked.open...vai/riv/dodaniDat	2013
http://linked.open...aciTvurceVysledku	Táborská, Eva Kantorová, Jana Gregorová, Jana Pěnčíková, Kristýna
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Masarykova univerzita / Lékařská fakulta
http://linked.open...dnocenehoVysledku	143131
http://linked.open...ai/riv/idVysledku	RIV/00216224:14110/12:00057370
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	Maceration; pressurised liquid extraction; Soxhlet extraction; benzo[c]phenanthridine alkaloids; Macleaya microcarpa (en)
http://linked.open.../riv/klicoveSlovo	Macleaya microcarpa Maceration benzo[c]phenanthridine alkaloids pressurised liquid extraction Soxhlet extraction
http://linked.open...odStatuVydavatele	US - Spojené státy americké
http://linked.open...ontrolniKodProRIV	[33E0B7269371]
http://linked.open...i/riv/nazevZdroje	Phytochemical Analysis
http://linked.open...in/vavai/riv/obor	CE
http://linked.open...ichTvurcuVysledku	4 (xsd:int)
http://linked.open...cetTvurcuVysledku	8 (xsd:int)
http://linked.open...vavai/riv/projekt	Plant sources of minor benzophenanthridine alkaloids and study of their interaction with DNA Alteration of the solvent properties of pressurized hot water: aqueous solubilities of macrocyclic additives Pressurized liquid extraction of high-value substances from plant materials
http://linked.open...UplatneniVysledku	2012
http://linked.open...v/svazekPeriodika	23
http://linked.open...iv/tvurceVysledku	Hohnová, Barbora Karásek, Pavel Roth, Michal Táborská, Eva Šťavíková, Lenka Kantorová, Jana Gregorová, Jana Pěnčíková, Kristýna
http://linked.open...ain/vavai/riv/wos	000307546500009
http://linked.open...n/vavai/riv/zamer	Moderní analytické techniky pro bioanalýzu, ekologii a nanotechnologie
issn	0958-0344
number of pages	6 (xsd:int)
http://bibframe.org/vocab/doi	10.1002/pca.2344
http://localhost/t...ganizacniJednotka	14110
is http://linked.open...avai/riv/vysledek of	Isolation of Quaternary Benzo[c] phenanthridine Alkaloids from Macleaya microcarpa (MAXIM.) FEDDE: Comparison of Maceration, Soxhlet Extraction and Pressurised Liquid Extraction

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