About: Simplified syntheses of the water-soluble chiral shift reagents Sm-(R)-pdta and Sm-(S)-pdta     Goto   Sponge   NotDistinct   Permalink

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Description
  • The chiral shift reagents Sm-(R)-pdta and Sm-(S)-pdta, which are based on (R)- or (S)-1,2-diaminopropane-N,N,N',N'-tetraacetic acid were synthesized from easily accessible compounds in three simple steps, which makes the method suitable for laboratory-scale production. In addition, a new and efficient method for the preparation of pure anhydrous (R)- or (S)-1,2-diaminopropane-N,N,N',N'-tetraacetic acid was developed.
  • The chiral shift reagents Sm-(R)-pdta and Sm-(S)-pdta, which are based on (R)- or (S)-1,2-diaminopropane-N,N,N',N'-tetraacetic acid were synthesized from easily accessible compounds in three simple steps, which makes the method suitable for laboratory-scale production. In addition, a new and efficient method for the preparation of pure anhydrous (R)- or (S)-1,2-diaminopropane-N,N,N',N'-tetraacetic acid was developed. (en)
Title
  • Simplified syntheses of the water-soluble chiral shift reagents Sm-(R)-pdta and Sm-(S)-pdta
  • Simplified syntheses of the water-soluble chiral shift reagents Sm-(R)-pdta and Sm-(S)-pdta (en)
skos:prefLabel
  • Simplified syntheses of the water-soluble chiral shift reagents Sm-(R)-pdta and Sm-(S)-pdta
  • Simplified syntheses of the water-soluble chiral shift reagents Sm-(R)-pdta and Sm-(S)-pdta (en)
skos:notation
  • RIV/00216208:11310/13:10174183!RIV14-MSM-11310___
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  • I
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  • 47
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  • 105134
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  • RIV/00216208:11310/13:10174183
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  • 2-diaminopropane; 1; samarium; pdta; Sm-pdta; chiral shift reagents; NMR (en)
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  • NL - Nizozemsko
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  • [E527318D339D]
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  • Tetrahedron Letters
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  • 54
http://linked.open...iv/tvurceVysledku
  • Hrubá, Lucie
  • Vaněk, Václav
  • Pícha, Jan
  • Jiráček, Jiří
  • Budešínský, Miloš
http://linked.open...ain/vavai/riv/wos
  • 000326430400002
issn
  • 0040-4039
number of pages
http://bibframe.org/vocab/doi
  • 10.1016/j.tetlet.2013.09.009
http://localhost/t...ganizacniJednotka
  • 11310
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