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| Description
| - The project is orientated to development and improvement of progressive methods of sample clean-up, preconcentration, separation, and detection for analyses in biochemistry and clinical and environmental chemistry. The research and development will be focused on the separation of analytes and sample matrix by electromigration across liquid phase boundaries and membranes in combination with preconcentration and separation effects of electromigration boundaries in capillary electrophoresis and with optimization of background electrolytes for sensitive on-line detection by mass spectrometry. New techniques will be developed allowing easier and more sensitive analyses of samples with complex matrices in research and application areas. (en)
- Projekt se bude zabývat vývojem a zdokonalováním progresivních metod úpravy vzorků, prekoncentrace, separace a detekce pro analýzy v biochemii, klinické chemii a chemii životního prostředí. Hlavním směrem budou separace analytů a matrice vzorku elektromigrací přes kapalná fázová rozhraní a membrány v následné kombinaci se zakoncentrovávacími a separačními efekty elektromigračních rozhraní v kapilární elektroforéze a s cílenou optimalizací základních elektrolytů pro citlivou on-line detekci pomocí hmotnostní spektrometrie. Aplikační využití bude orientováno na snazší a citlivější analýzy vzorků se složitými matricemi.
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| Title
| - Progressive methods of sample clean-up, preconcentration, separation and detection in biochemical, clinical and environmental analyses (en)
- Progresivní metody úpravy vzorků, prekoncentrace, separace a detekce pro analýzy v biochemii a klinické a environmentální chemii
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| skos:notation
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| http://linked.open...avai/cep/aktivita
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| http://linked.open...kovaStatniPodpora
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| http://linked.open...ep/celkoveNaklady
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| http://linked.open...datumDodatniDoRIV
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| http://linked.open...i/cep/druhSouteze
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| http://linked.open...ep/duvernostUdaju
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| http://linked.open.../cep/fazeProjektu
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| http://linked.open...ai/cep/hlavniObor
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| http://linked.open...hodnoceniProjektu
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| http://linked.open...vai/cep/kategorie
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| http://linked.open.../cep/klicovaSlova
| - capillary; zone; electrophoresis; concentrating; analytical; methods; phase; and; membrane; boundaries (en)
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| http://linked.open...ep/partnetrHlavni
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| http://linked.open...inujicichPrijemcu
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| http://linked.open...cep/pocetPrijemcu
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| http://linked.open...ocetSpoluPrijemcu
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| http://linked.open.../pocetVysledkuRIV
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| http://linked.open...enychVysledkuVRIV
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| http://linked.open...lneniVMinulemRoce
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| http://linked.open.../prideleniPodpory
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| http://linked.open...iciPoslednihoRoku
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| http://linked.open...atUdajeProjZameru
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| http://linked.open.../vavai/cep/soutez
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| http://linked.open...usZobrazovaneFaze
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| http://linked.open...ai/cep/typPojektu
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| http://linked.open...ep/ukonceniReseni
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| http://linked.open.../cep/vedlejsiObor
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| http://linked.open...ep/zahajeniReseni
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| http://linked.open...jektu+dodavatelem
| - Odborný přínos projektu je mimořádně vysoký, byly vyvinuty nové analytické metody. Charakteristika výsledků řešiteli je adekvátní. Výsledky projektu jsou významné i pro jiné obory; na řešení úkolů projektu se podíleli i studenti. Publikační výstupy grantu jsou velmi hodnotné: 23 prací v tzv.. impaktovaných časopisech a řada přednášek na mezinárodních symposiích. Nedostatky se nevyskytly. (cs)
- Professional quality is extremely high, new methods have been developed. Characterization of the results by the investigators is adequate. The results are important also in other fields; students participated in the project solution. Publication outputs are of great value: 23 papers in impacted journals, lectures at international symposia. No formal shortcomings occurred. (en)
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| http://linked.open...tniCyklusProjektu
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| http://linked.open.../cep/klicoveSlovo
| - capillary
- analytical
- and
- concentrating
- electrophoresis
- membrane
- methods
- phase
- zone
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| is http://linked.open...vavai/riv/projekt
of | - A simple sample pretreatment device with supported liquid membrane for direct injection of untreated body fluids and in-line coupling to a commercial CE instrument
- Contactless conductivity detection for analytical techniques: Developments from 2010 to 2012
- Electromembrane extraction of heavy metal cations followed by capillary electrophoresis with capacitively coupled contactless conductivity detection
- Electromembrane extraction of amino acids from body fluids followed by capillary electrophoresis with capacitively coupled contactless conductivity detection
- Focusing of alkali earth metals in ligand step gradient.
- Use of disposable open tubular ion exchange pre-columns for in-line clean-up of serum and plasma samples prior to capillary electrophoretic analysis of inorganic cations
- Trace determination of perchlorate using electromembrane extraction and capillary electrophoresis with capacitively coupled contactless conductivity detection
- A simple sample pretreatment device with supported liquid membrane for direct injection of untreated body fluids and in-line coupling to a commercial capillary electrophoresis instrument
- Capillary electrophoresis with capacitively coupled contactless conductivity detection: A universal tool for the determination of supported liquid membrane selectivity in electromembrane extraction of complex samples
- Advanced electrolyte tuning and selectivity enhancement for highly sensitive analysis of cations by capillary ITP-ESI MS
- Contemporary sample stacking in analytical electrophoresis
- Recent progress in analytical capillary isotachophoresis
- Method for on-line pre-concentration and analysis of heavy metals using ligand step gradient focusing in combination with ITP
- Direct analysis of formate in human plasma, serum and whole blood by in-line coupling of microdialysis to capillary electrophoresis for rapid diagnosis of methanol poisoning
- Effective pre-concentration and analysis of heavy metals using ligand step gradient focusing in combination with ITP (LSGF-ITP)
- Effective pre-concentration and analysis of heavy metals using ligand step gradient focusing in combination with ITP (LSGF-ITP).
- Electromembrane extraction using stabilized constant d.c. electric current — A simple tool for improvement of extraction performance
- Electrokinetic injection across supported liquid membranes: New sample pretreatment technique for online coupling to capillary electrophoresis. Direct analysis of perchlorate in biological samples
- Highly sensitive determination of cationic pesticides in orange juice by capillary isotachophoresis-electrospray ionization - mass spectrometry with advanced electrolyte tuning
- Selective focusing and analysis of Na+,Ca2+,Mg2+,Mn2+,Cd2+,Zn2+,Ni2+,Pb2+,Cu2+ using ligand step gradient focusing in combination with ITP (LSGF-ITP).
- Analysis of inorganic cations in biological samples by the combination of micro-electrodialysis and capillary electrophoresis with capacitively coupled contactless conductivity detection
- Capacitively coupled contactless conductivity detection for microseparation techniques – recent developments
- Recent advances in CE-MS: Synergy of wet chemistry and instrumentation innovations
- Rapid and simple pretreatment of human body fluids using electromembrane extraction across supported liquid membrane for capillary electrophoretic determination of lithium
- On-line coupling of a clean-up device with supported liquid membrane to capillary electrophoresis for direct injection and analysis of serum and plasma samples
- Important electromigration effects of carbon dioxide in capillary electrophoresis at high pH
- Analysis of 5-methyltetrahydrofolate in human blood, serum and urine by on-line coupling of capillary isotachophoresis and zone electrophoresis
- IZOELEKTRICKÁ FOKUSACE VE SKOKOVÉM GRADIENTU pH
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| is http://linked.open...vavai/cep/projekt
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