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Description
| - In this study, potential sweep technique and controlled potential electrolysis were used to analyze the electrochemical oxidation of glycerin in a three electrode system using platinum as a working electrode. Electrochemical experiments were performed at different concentrations of glycerin and manganese dioxide (0.015-0.124 M) to analyze the reaction order of reactant and oxidant.Voltammograms were studied at different positive and negative potential limits (-1.5 to 1.5 V vs Ag/AgCl), sweep rates (0.01 to 0.08 V/s) and temperatures (27 to 60 °C). The influence of each parameter on the voltammogram shape is discussed. Prolonged electrolysis at controlled potential yield glyceraldehyde, glyceric acid and glycolid acid as the main products.
- In this study, potential sweep technique and controlled potential electrolysis were used to analyze the electrochemical oxidation of glycerin in a three electrode system using platinum as a working electrode. Electrochemical experiments were performed at different concentrations of glycerin and manganese dioxide (0.015-0.124 M) to analyze the reaction order of reactant and oxidant.Voltammograms were studied at different positive and negative potential limits (-1.5 to 1.5 V vs Ag/AgCl), sweep rates (0.01 to 0.08 V/s) and temperatures (27 to 60 °C). The influence of each parameter on the voltammogram shape is discussed. Prolonged electrolysis at controlled potential yield glyceraldehyde, glyceric acid and glycolid acid as the main products. (en)
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Title
| - Electrooxidation of Glycerin by Potential Sweep Technique and Controlled Potential Electrolysis
- Electrooxidation of Glycerin by Potential Sweep Technique and Controlled Potential Electrolysis (en)
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skos:prefLabel
| - Electrooxidation of Glycerin by Potential Sweep Technique and Controlled Potential Electrolysis
- Electrooxidation of Glycerin by Potential Sweep Technique and Controlled Potential Electrolysis (en)
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skos:notation
| - RIV/70883521:28140/14:43871536!RIV15-MSM-28140___
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http://linked.open...avai/riv/aktivita
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http://linked.open...avai/riv/aktivity
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http://linked.open...iv/cisloPeriodika
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http://linked.open...vai/riv/dodaniDat
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http://linked.open...aciTvurceVysledku
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http://linked.open.../riv/druhVysledku
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http://linked.open...iv/duvernostUdaju
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http://linked.open...titaPredkladatele
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http://linked.open...dnocenehoVysledku
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http://linked.open...ai/riv/idVysledku
| - RIV/70883521:28140/14:43871536
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http://linked.open...riv/jazykVysledku
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http://linked.open.../riv/klicovaSlova
| - glycerin, potential sweep, controlled potential, anodic oxidation, platinum electrode (en)
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http://linked.open.../riv/klicoveSlovo
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http://linked.open...odStatuVydavatele
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http://linked.open...ontrolniKodProRIV
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http://linked.open...i/riv/nazevZdroje
| - International Journal of Electrochemical Sciences
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http://linked.open...in/vavai/riv/obor
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http://linked.open...ichTvurcuVysledku
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http://linked.open...cetTvurcuVysledku
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http://linked.open...vavai/riv/projekt
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http://linked.open...UplatneniVysledku
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http://linked.open...v/svazekPeriodika
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http://linked.open...iv/tvurceVysledku
| - Kolomazník, Karel
- Slavík, Roman
- Beltrán Prieto, Juan Carlos
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http://linked.open...ain/vavai/riv/wos
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issn
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number of pages
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http://localhost/t...ganizacniJednotka
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