About: C60 Fullerene derivative: Preparation of a water-soluble fullerene derivative in reaction with peracetic acid     Goto   Sponge   NotDistinct   Permalink

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  • Water-soluble C60 derivative was obtained by the reaction of the C60 fullerene with the peracetic acid followed by hydrolysis; the acid was used as a strong oxidizing agent to provide the oxygen needed to create the C=C double bond of the six-member ring of fullerene cage. Fullerene solubility, defined as a condition in which no more particles settle or visibly cluster, was determined to be 400 mg/liter. Visual comparison suffices to see the differences in solubility between the starting form and the modified form of C60. TEM (100 and 300 kV) and SEM microscopy results found the starting C60 modified both in the homogeneity of sizes of the irregular complexes and in their very sizes and crystallinity. Properties observed in the modified sample obviously facilitate the process of solving and that of obtaining a homogenous aquatic solution or suspension containing crystals of microscopic sizes.
  • Water-soluble C60 derivative was obtained by the reaction of the C60 fullerene with the peracetic acid followed by hydrolysis; the acid was used as a strong oxidizing agent to provide the oxygen needed to create the C=C double bond of the six-member ring of fullerene cage. Fullerene solubility, defined as a condition in which no more particles settle or visibly cluster, was determined to be 400 mg/liter. Visual comparison suffices to see the differences in solubility between the starting form and the modified form of C60. TEM (100 and 300 kV) and SEM microscopy results found the starting C60 modified both in the homogeneity of sizes of the irregular complexes and in their very sizes and crystallinity. Properties observed in the modified sample obviously facilitate the process of solving and that of obtaining a homogenous aquatic solution or suspension containing crystals of microscopic sizes. (en)
Title
  • C60 Fullerene derivative: Preparation of a water-soluble fullerene derivative in reaction with peracetic acid
  • C60 Fullerene derivative: Preparation of a water-soluble fullerene derivative in reaction with peracetic acid (en)
skos:prefLabel
  • C60 Fullerene derivative: Preparation of a water-soluble fullerene derivative in reaction with peracetic acid
  • C60 Fullerene derivative: Preparation of a water-soluble fullerene derivative in reaction with peracetic acid (en)
skos:notation
  • RIV/70565813:_____/09:#0000188!RIV10-SUJ-70565813
http://linked.open...avai/riv/aktivita
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  • Z(SUJ200401)
http://linked.open...vai/riv/dodaniDat
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  • 308957
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  • RIV/70565813:_____/09:#0000188
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  • Fullerene Derivative; Hydroxylation; Oxidation; Electron Microscopy; Microstructure (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...ontrolniKodProRIV
  • [1B330D2A0FC0]
http://linked.open...v/mistoKonaniAkce
  • Rožnov pod Radhoštěm, Česká republika
http://linked.open...i/riv/mistoVydani
  • Ostrava, CZ, EU
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  • Conference proceedings, Nanocon 2009
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
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http://linked.open...UplatneniVysledku
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  • Klouda, Karel
  • Beranová, Eva
http://linked.open...vavai/riv/typAkce
http://linked.open...ain/vavai/riv/wos
  • 000277025600021
http://linked.open.../riv/zahajeniAkce
http://linked.open...n/vavai/riv/zamer
number of pages
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  • 2009 Tanger Ltd., Keltickova 62, 710 00 Slezska Ostrava, CZ
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  • 978-80-87294-13-0
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