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Description
  • Determination of 236U/238U at natural ratios using accelerator mass spectrometry (AMS) requires overall purity of each step in the sample preparation procedures which are complex and include various chemicals. Therefore, the simplification of the procedures is desirable and can be done by implementing other effective separation materials. Among the prospective sorption materials, hydrated titanium dioxides showed promising properties for uranium extraction from various water samples. This paper shows the preparation of several titanium based sorption materials using an organic precursor and their characterization with several techniques in order to analyse crystal structure (XRPD, SEM, HRTEM, SAED) and residues of organic compounds (TG analysis and IR spectroscopy) and to quantify their sorption properties towards uranium. The practical sorption capacity of one of the prepared materials was as high as 260 mg of uranium per gram. AMS measurements showed that it is possible to prepare sufficiently pure titanium dioxides for the determination of 236U/238U ratio
  • Determination of 236U/238U at natural ratios using accelerator mass spectrometry (AMS) requires overall purity of each step in the sample preparation procedures which are complex and include various chemicals. Therefore, the simplification of the procedures is desirable and can be done by implementing other effective separation materials. Among the prospective sorption materials, hydrated titanium dioxides showed promising properties for uranium extraction from various water samples. This paper shows the preparation of several titanium based sorption materials using an organic precursor and their characterization with several techniques in order to analyse crystal structure (XRPD, SEM, HRTEM, SAED) and residues of organic compounds (TG analysis and IR spectroscopy) and to quantify their sorption properties towards uranium. The practical sorption capacity of one of the prepared materials was as high as 260 mg of uranium per gram. AMS measurements showed that it is possible to prepare sufficiently pure titanium dioxides for the determination of 236U/238U ratio (en)
Title
  • Preparation of pure TiO2 sorption material
  • Preparation of pure TiO2 sorption material (en)
skos:prefLabel
  • Preparation of pure TiO2 sorption material
  • Preparation of pure TiO2 sorption material (en)
skos:notation
  • RIV/68407700:21340/14:00214127!RIV15-MSM-21340___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • S
http://linked.open...iv/cisloPeriodika
  • 3
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 39050
http://linked.open...ai/riv/idVysledku
  • RIV/68407700:21340/14:00214127
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • AMS; Sorption; Titanium dioxide; Uranium (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • HU - Maďarsko
http://linked.open...ontrolniKodProRIV
  • [E17A66359F5A]
http://linked.open...i/riv/nazevZdroje
  • Journal of Radioanalytical and Nuclear Chemistry
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 300
http://linked.open...iv/tvurceVysledku
  • Špendlíková, Irena
  • Němec, Mojmír
  • Steier, P.
  • Mičolová, Petra
  • Raindl, J.
http://linked.open...ain/vavai/riv/wos
  • 000335673800030
issn
  • 0236-5731
number of pages
http://bibframe.org/vocab/doi
  • 10.1007/s10967-014-3061-x
http://localhost/t...ganizacniJednotka
  • 21340
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