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Description
| - A new mononuclear octahedral cobalt(III) Schiff base complex has been synthesized and characterized by elemental analyses (CHN) and FT-IR spectroscopy and used as precursor for preparation of Co3O4 nanoparticles. The crystal structure of this compound has been determined by single-crystal X-ray diffraction. The coordination sphere about cobalt(III) ion consists of three phenolato oxygens and three imino nitrogen atoms from three Schiff base ligands, thus forming a distorted octahedral geometry. Each Schiff base ligand acts as a chelate using phenolato oxygen and imino nitrogen. Subsequently, pure phase Co3O4 nanoparticles, with an average size in the range 10–20 nm, were obtained by solid-state thermal decomposition of the synthesized complex at 450 degC under air atmosphere for 3 h.
- A new mononuclear octahedral cobalt(III) Schiff base complex has been synthesized and characterized by elemental analyses (CHN) and FT-IR spectroscopy and used as precursor for preparation of Co3O4 nanoparticles. The crystal structure of this compound has been determined by single-crystal X-ray diffraction. The coordination sphere about cobalt(III) ion consists of three phenolato oxygens and three imino nitrogen atoms from three Schiff base ligands, thus forming a distorted octahedral geometry. Each Schiff base ligand acts as a chelate using phenolato oxygen and imino nitrogen. Subsequently, pure phase Co3O4 nanoparticles, with an average size in the range 10–20 nm, were obtained by solid-state thermal decomposition of the synthesized complex at 450 degC under air atmosphere for 3 h. (en)
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Title
| - Synthesis of new cobalt(III) Schiff base complex: a new precursor for preparation Co3O4 nanoparticles via solid-state thermal decomposition
- Synthesis of new cobalt(III) Schiff base complex: a new precursor for preparation Co3O4 nanoparticles via solid-state thermal decomposition (en)
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skos:prefLabel
| - Synthesis of new cobalt(III) Schiff base complex: a new precursor for preparation Co3O4 nanoparticles via solid-state thermal decomposition
- Synthesis of new cobalt(III) Schiff base complex: a new precursor for preparation Co3O4 nanoparticles via solid-state thermal decomposition (en)
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skos:notation
| - RIV/68378271:_____/14:00435001!RIV15-AV0-68378271
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http://linked.open...avai/riv/aktivita
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http://linked.open...avai/riv/aktivity
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http://linked.open...iv/cisloPeriodika
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http://linked.open...vai/riv/dodaniDat
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http://linked.open...aciTvurceVysledku
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http://linked.open.../riv/druhVysledku
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http://linked.open...iv/duvernostUdaju
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http://linked.open...titaPredkladatele
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http://linked.open...dnocenehoVysledku
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http://linked.open...ai/riv/idVysledku
| - RIV/68378271:_____/14:00435001
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http://linked.open...riv/jazykVysledku
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http://linked.open.../riv/klicovaSlova
| - cobalt(III) Schiff base complex; single-crystal structure analysis; Co3O4 nanoparticles; SEM; TEM (en)
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http://linked.open.../riv/klicoveSlovo
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http://linked.open...odStatuVydavatele
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http://linked.open...ontrolniKodProRIV
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http://linked.open...i/riv/nazevZdroje
| - Journal of Molecular Structure
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http://linked.open...in/vavai/riv/obor
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http://linked.open...ichTvurcuVysledku
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http://linked.open...cetTvurcuVysledku
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http://linked.open...UplatneniVysledku
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http://linked.open...v/svazekPeriodika
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http://linked.open...iv/tvurceVysledku
| - Dušek, Michal
- Fejfarová, Karla
- Khalaji, A. D.
- Nikookar, M.
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http://linked.open...ain/vavai/riv/wos
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issn
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number of pages
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http://bibframe.org/vocab/doi
| - 10.1016/j.molstruc.2014.04.043
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