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  • A new mononuclear octahedral cobalt(III) Schiff base complex has been synthesized and characterized by elemental analyses (CHN) and FT-IR spectroscopy and used as precursor for preparation of Co3O4 nanoparticles. The crystal structure of this compound has been determined by single-crystal X-ray diffraction. The coordination sphere about cobalt(III) ion consists of three phenolato oxygens and three imino nitrogen atoms from three Schiff base ligands, thus forming a distorted octahedral geometry. Each Schiff base ligand acts as a chelate using phenolato oxygen and imino nitrogen. Subsequently, pure phase Co3O4 nanoparticles, with an average size in the range 10–20 nm, were obtained by solid-state thermal decomposition of the synthesized complex at 450 degC under air atmosphere for 3 h.
  • A new mononuclear octahedral cobalt(III) Schiff base complex has been synthesized and characterized by elemental analyses (CHN) and FT-IR spectroscopy and used as precursor for preparation of Co3O4 nanoparticles. The crystal structure of this compound has been determined by single-crystal X-ray diffraction. The coordination sphere about cobalt(III) ion consists of three phenolato oxygens and three imino nitrogen atoms from three Schiff base ligands, thus forming a distorted octahedral geometry. Each Schiff base ligand acts as a chelate using phenolato oxygen and imino nitrogen. Subsequently, pure phase Co3O4 nanoparticles, with an average size in the range 10–20 nm, were obtained by solid-state thermal decomposition of the synthesized complex at 450 degC under air atmosphere for 3 h. (en)
Title
  • Synthesis of new cobalt(III) Schiff base complex: a new precursor for preparation Co3O4 nanoparticles via solid-state thermal decomposition
  • Synthesis of new cobalt(III) Schiff base complex: a new precursor for preparation Co3O4 nanoparticles via solid-state thermal decomposition (en)
skos:prefLabel
  • Synthesis of new cobalt(III) Schiff base complex: a new precursor for preparation Co3O4 nanoparticles via solid-state thermal decomposition
  • Synthesis of new cobalt(III) Schiff base complex: a new precursor for preparation Co3O4 nanoparticles via solid-state thermal decomposition (en)
skos:notation
  • RIV/68378271:_____/14:00435001!RIV15-AV0-68378271
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  • RIV/68378271:_____/14:00435001
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  • cobalt(III) Schiff base complex; single-crystal structure analysis; Co3O4 nanoparticles; SEM; TEM (en)
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  • NL - Nizozemsko
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  • [0478724C53AE]
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  • Journal of Molecular Structure
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  • 1071
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  • Dušek, Michal
  • Fejfarová, Karla
  • Khalaji, A. D.
  • Nikookar, M.
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  • 000338821800002
issn
  • 0022-2860
number of pages
http://bibframe.org/vocab/doi
  • 10.1016/j.molstruc.2014.04.043
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