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  • A new non-solution mediated approach to the synthesis of iron oxide nanoparticles directly from solid FeCl2salt precursors developed. Rapid, simple and scalable method. Structural properties and the phase of the resulting iron oxide particles has been determined by a range of methods including XRD, FT-IR and Mössbauer spectroscopy, and the phase is shown to be maghemite (γ-Fe2O3). Iron oxide particles magnetic properties measured using SQUID, confirming superparamagnetic behaviour of the powder and a saturation magnetization of 53.0 emu g-1 at 300 K. Aqueous dispersions at increasing concentrations prepared and their heating rate under a 400 kHz alternating magnetic field measured. The specific absorption rate (SAR) of the iron oxide was found to be 84.8 W g-1, which makes the material suitable for the formulation of ferrofluids or ferrogels with RF heating properties.
  • A new non-solution mediated approach to the synthesis of iron oxide nanoparticles directly from solid FeCl2salt precursors developed. Rapid, simple and scalable method. Structural properties and the phase of the resulting iron oxide particles has been determined by a range of methods including XRD, FT-IR and Mössbauer spectroscopy, and the phase is shown to be maghemite (γ-Fe2O3). Iron oxide particles magnetic properties measured using SQUID, confirming superparamagnetic behaviour of the powder and a saturation magnetization of 53.0 emu g-1 at 300 K. Aqueous dispersions at increasing concentrations prepared and their heating rate under a 400 kHz alternating magnetic field measured. The specific absorption rate (SAR) of the iron oxide was found to be 84.8 W g-1, which makes the material suitable for the formulation of ferrofluids or ferrogels with RF heating properties. (en)
Title
  • Vapor phase approach for iron oxide nanoparticle synthesis from solid precursors
  • Vapor phase approach for iron oxide nanoparticle synthesis from solid precursors (en)
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  • Vapor phase approach for iron oxide nanoparticle synthesis from solid precursors
  • Vapor phase approach for iron oxide nanoparticle synthesis from solid precursors (en)
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  • RIV/68378271:_____/13:00394513!RIV14-AV0-68378271
http://linked.open...avai/riv/aktivita
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  • 113609
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  • RIV/68378271:_____/13:00394513
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  • nanoparticle; maghemite; radiofrequency heating; superparamagnetism; saturation magnetisation (en)
http://linked.open.../riv/klicoveSlovo
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  • US - Spojené státy americké
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  • [0BD9A7570AEE]
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  • Journal of Solid State Chemistry
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  • 200
http://linked.open...iv/tvurceVysledku
  • Svoboda, P.
  • Šantavá, Eva
  • Singh, M.
  • Ulbrich, P.
  • Štěpánek, F.
  • Prokopec, V.
http://linked.open...ain/vavai/riv/wos
  • 000317158000023
issn
  • 0022-4596
number of pages
http://bibframe.org/vocab/doi
  • 10.1016/j.jssc.2013.01.037
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