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  • Two samples of nanopowders containing superparamagnetic Fe3C and Fe3O4/gamma-Fe2O3 particles and carbon black were synthesized by the method of laser-induced homogeneous pyrolysis of gaseous precursors. Both were characterized by XRD, HR-TEM, Mössbauer spectrometry and standard magnetic measurements. The mean crystallite size of Fe3C was 3 nm for the first sample and 10 nm for the second sample. Fe3C phase in both samples exhibited reduced Curie temperature and smeared ferromagnetic-paramagnetic transition. After annealing of the samples at 800°C for 30min the Curie temperature of the recrystallized Fe3C phase in both samples was 214°C (standard bulk value).
  • Two samples of nanopowders containing superparamagnetic Fe3C and Fe3O4/gamma-Fe2O3 particles and carbon black were synthesized by the method of laser-induced homogeneous pyrolysis of gaseous precursors. Both were characterized by XRD, HR-TEM, Mössbauer spectrometry and standard magnetic measurements. The mean crystallite size of Fe3C was 3 nm for the first sample and 10 nm for the second sample. Fe3C phase in both samples exhibited reduced Curie temperature and smeared ferromagnetic-paramagnetic transition. After annealing of the samples at 800°C for 30min the Curie temperature of the recrystallized Fe3C phase in both samples was 214°C (standard bulk value). (en)
Title
  • Nanopowders with superparamagnetic Fe3C particles and their annealing behaviour
  • Nanopowders with superparamagnetic Fe3C particles and their annealing behaviour (en)
skos:prefLabel
  • Nanopowders with superparamagnetic Fe3C particles and their annealing behaviour
  • Nanopowders with superparamagnetic Fe3C particles and their annealing behaviour (en)
skos:notation
  • RIV/68081723:_____/10:00354295!RIV11-MSM-68081723
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(1M0512), P(GA202/08/0178), Z(AV0Z20410507)
http://linked.open...iv/cisloPeriodika
  • 6-7
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  • 273634
http://linked.open...ai/riv/idVysledku
  • RIV/68081723:_____/10:00354295
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • Fe3C; nanocomposite; magnetic measurements; Mössbauer spectroscopy; superparamagnetism (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • GB - Spojené království Velké Británie a Severního Irska
http://linked.open...ontrolniKodProRIV
  • [160499DDF7BE]
http://linked.open...i/riv/nazevZdroje
  • Surface and Interface Analysis
http://linked.open...in/vavai/riv/obor
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http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 42
http://linked.open...iv/tvurceVysledku
  • David, Bohumil
  • Schneeweiss, Oldřich
  • Pizúrová, Naděžda
  • Alexandrescu, R.
  • Dumitrache, F.
  • Fleaca, C.
http://linked.open...ain/vavai/riv/wos
  • 000281149700054
http://linked.open...n/vavai/riv/zamer
issn
  • 0142-2421
number of pages
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