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Description
| - We prepared Mg-Fe and Mg-Fe-Ni nanocomposites using spark synthesis of pure Mg, and Fe or permalloy (Ni3Fe) electrodes. The magnetic separation and sedimentation treatments were used for separation of nanocrystaline parts from the as-prepared powders. In the Mg-Fe sample, a-Fe, Fe in Mg, and FeO phases were determined using the Mössbauer phase analysis, and Mg, MgO, and a-Fe by the x-ray diffraction measurements. The Fe in Mg phase with approx. 8at.% Fe is a new metastable phase not described in equilibrium phase diagram handbooks until now. Its temperature dependence of magnetization showed spin-glass like behaviour of the sample. An annealing in vacuum (10-3 Pa) or in the protective atmosphere (H2) caused transformation of the Fe in Mg phase into a-Fe. With increasing a-Fe content an increase of the FeO was observed. The Mg-Fe-Ni nanocomposite exhibits similar behaviour and phase composition but the Ni3Fe phase was replaced the a-Fe and different features of the Fe(Ni) in Mg phase were observed. B
- We prepared Mg-Fe and Mg-Fe-Ni nanocomposites using spark synthesis of pure Mg, and Fe or permalloy (Ni3Fe) electrodes. The magnetic separation and sedimentation treatments were used for separation of nanocrystaline parts from the as-prepared powders. In the Mg-Fe sample, a-Fe, Fe in Mg, and FeO phases were determined using the Mössbauer phase analysis, and Mg, MgO, and a-Fe by the x-ray diffraction measurements. The Fe in Mg phase with approx. 8at.% Fe is a new metastable phase not described in equilibrium phase diagram handbooks until now. Its temperature dependence of magnetization showed spin-glass like behaviour of the sample. An annealing in vacuum (10-3 Pa) or in the protective atmosphere (H2) caused transformation of the Fe in Mg phase into a-Fe. With increasing a-Fe content an increase of the FeO was observed. The Mg-Fe-Ni nanocomposite exhibits similar behaviour and phase composition but the Ni3Fe phase was replaced the a-Fe and different features of the Fe(Ni) in Mg phase were observed. B (en)
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Title
| - Preparation and properties of Mg-Fe and Mg-Ni-Fe nanocomposites.
- Preparation and properties of Mg-Fe and Mg-Ni-Fe nanocomposites. (en)
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skos:prefLabel
| - Preparation and properties of Mg-Fe and Mg-Ni-Fe nanocomposites.
- Preparation and properties of Mg-Fe and Mg-Ni-Fe nanocomposites. (en)
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skos:notation
| - RIV/68081723:_____/01:07013270!RIV/2003/AV0/A07003/N
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http://linked.open.../vavai/riv/strany
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http://linked.open...avai/riv/aktivita
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http://linked.open...avai/riv/aktivity
| - P(GA106/99/0183), P(GA202/01/0668), P(ME 209), Z(AV0Z1010914), Z(AV0Z2041904)
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http://linked.open...vai/riv/dodaniDat
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http://linked.open...aciTvurceVysledku
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http://linked.open.../riv/druhVysledku
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http://linked.open...iv/duvernostUdaju
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http://linked.open...titaPredkladatele
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http://linked.open...dnocenehoVysledku
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http://linked.open...ai/riv/idVysledku
| - RIV/68081723:_____/01:07013270
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http://linked.open...riv/jazykVysledku
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http://linked.open.../riv/klicovaSlova
| - nanocrystals; magnetism; Mössbauer spectroscopy (en)
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http://linked.open.../riv/klicoveSlovo
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http://linked.open...ontrolniKodProRIV
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http://linked.open...v/mistoKonaniAkce
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http://linked.open...i/riv/mistoVydani
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http://linked.open...i/riv/nazevZdroje
| - 11th Czech and Slovak Conference on Magnetism CSMAG'01 - Programme & Abstracts.
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http://linked.open...in/vavai/riv/obor
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http://linked.open...ichTvurcuVysledku
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http://linked.open...cetTvurcuVysledku
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http://linked.open...ocetUcastnikuAkce
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http://linked.open...nichUcastnikuAkce
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http://linked.open...vavai/riv/projekt
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http://linked.open...UplatneniVysledku
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http://linked.open...iv/tvurceVysledku
| - Schneeweiss, Oldřich
- Šebek, Josef
- Jirásková, Yvonna
- Lin, S.
- Yao, X.
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http://linked.open...vavai/riv/typAkce
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http://linked.open.../riv/zahajeniAkce
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http://linked.open...n/vavai/riv/zamer
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number of pages
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http://purl.org/ne...btex#hasPublisher
| - Šafarik University Košice
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