About: High pressure modification of the simple automated liquid chromatographic system for splitless nano column gradient separations

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	Our simple liquid chromatographic system for splitless gradient nanocolumn separations at backpressure up to 50 bars was modified to run analysis under the pressure up to 300 bars. Programmable syringe pump was equipped with a 250-L high-pressure syringe and mobile phase gradients were created and stored in relatively long capillary. Available linear gradients of volumes from 5 to 50 L traced by uracil are presented. Sample introduction was performed as separate step and real large volume of sample (tens of microliters) could be injected and preconcentrated on-column. Relative standard deviation of retention times and peak areas were received (RSD < 0.3 % and RSD < 5 % respectively). Our simple liquid chromatographic system for splitless gradient nanocolumn separations at backpressure up to 50 bars was modified to run analysis under the pressure up to 300 bars. Programmable syringe pump was equipped with a 250-L high-pressure syringe and mobile phase gradients were created and stored in relatively long capillary. Available linear gradients of volumes from 5 to 50 L traced by uracil are presented. Sample introduction was performed as separate step and real large volume of sample (tens of microliters) could be injected and preconcentrated on-column. Relative standard deviation of retention times and peak areas were received (RSD < 0.3 % and RSD < 5 % respectively). (en)
Title	High pressure modification of the simple automated liquid chromatographic system for splitless nano column gradient separations High pressure modification of the simple automated liquid chromatographic system for splitless nano column gradient separations (en)
skos:prefLabel	High pressure modification of the simple automated liquid chromatographic system for splitless nano column gradient separations High pressure modification of the simple automated liquid chromatographic system for splitless nano column gradient separations (en)
skos:notation	RIV/68081715:_____/13:00422993!RIV14-MV0-68081715
http://linked.open...avai/riv/aktivita	I P
http://linked.open...avai/riv/aktivity	I, P(VG20112015021)
http://linked.open...vai/riv/dodaniDat	2014
http://linked.open...aciTvurceVysledku	Kahle, Vladislav Šesták, Jozef
http://linked.open.../riv/druhVysledku	D - Článek ve sborníku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Ústav analytické chemie AV ČR, v. v. i.
http://linked.open...dnocenehoVysledku	77356
http://linked.open...ai/riv/idVysledku	RIV/68081715:_____/13:00422993
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	liquid chromatography; nano column gradient separations; gradient separation (en)
http://linked.open.../riv/klicoveSlovo	liquid chromatography gradient separation nano column gradient separations
http://linked.open...ontrolniKodProRIV	[0A9C2C010F25]
http://linked.open...v/mistoKonaniAkce	Brno
http://linked.open...i/riv/mistoVydani	Praha
http://linked.open...i/riv/nazevZdroje	Chemické Listy. Roč. 107, Issue s3.
http://linked.open...in/vavai/riv/obor	CB
http://linked.open...ichTvurcuVysledku	2 (xsd:int)
http://linked.open...cetTvurcuVysledku	2 (xsd:int)
http://linked.open...vavai/riv/projekt	Development of instrumental methods for rapid detection and identification of biological agens in field samples
http://linked.open...UplatneniVysledku	2013
http://linked.open...iv/tvurceVysledku	Šesták, Jozef Kahle, Vladislav
http://linked.open...vavai/riv/typAkce	WRD - Světová
http://linked.open...ain/vavai/riv/wos	000328730800063
http://linked.open.../riv/zahajeniAkce	2013-11-12 (xsd:date)
issn	1213-7103
number of pages	3 (xsd:int)
http://purl.org/ne...btex#hasPublisher	Česká společnost chemická

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