About: Preparation of silicon oxycarbide composites toughened by inorganic fibers via pyrolysis of precursor siloxane composites     Goto   Sponge   NotDistinct   Permalink

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Description
  • The optimization of silicon oxycarbide (SiOC) synthesis (sol-gel/pyrolysis) is described, starting from methyltriethoxysilane, dimethyldiethoxysilane, tetraethoxysilane, ethyltriethoxysilane and propyltriethoxysilane. Variation of final elemental composition was tested via change of monomer ratios and combinations. The main aim was to achieve low weight losses during cure and pyrolysis and high micromechanical properties. Gas chromatography and mass spectroscopy was used to analyse the by-products of cure and pyrolysis, indicating a prominent role of cyclosiloxane and polyhedral oligomeric silsesquioxane (POSS) oligomers. Best results were obtained with high contents of methyltriethoxysilane in the monomers mixture.
  • The optimization of silicon oxycarbide (SiOC) synthesis (sol-gel/pyrolysis) is described, starting from methyltriethoxysilane, dimethyldiethoxysilane, tetraethoxysilane, ethyltriethoxysilane and propyltriethoxysilane. Variation of final elemental composition was tested via change of monomer ratios and combinations. The main aim was to achieve low weight losses during cure and pyrolysis and high micromechanical properties. Gas chromatography and mass spectroscopy was used to analyse the by-products of cure and pyrolysis, indicating a prominent role of cyclosiloxane and polyhedral oligomeric silsesquioxane (POSS) oligomers. Best results were obtained with high contents of methyltriethoxysilane in the monomers mixture. (en)
Title
  • Preparation of silicon oxycarbide composites toughened by inorganic fibers via pyrolysis of precursor siloxane composites
  • Preparation of silicon oxycarbide composites toughened by inorganic fibers via pyrolysis of precursor siloxane composites (en)
skos:prefLabel
  • Preparation of silicon oxycarbide composites toughened by inorganic fibers via pyrolysis of precursor siloxane composites
  • Preparation of silicon oxycarbide composites toughened by inorganic fibers via pyrolysis of precursor siloxane composites (en)
skos:notation
  • RIV/67985891:_____/11:00362897!RIV12-AV0-67985891
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(GA106/09/1101), Z(AV0Z20410507), Z(AV0Z30460519), Z(AV0Z40500505)
http://linked.open...iv/cisloPeriodika
  • 2
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 223101
http://linked.open...ai/riv/idVysledku
  • RIV/67985891:_____/11:00362897
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • silicon oxycarbide; SiOC; siloxane (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • PL - Polská republika
http://linked.open...ontrolniKodProRIV
  • [B644665C3524]
http://linked.open...i/riv/nazevZdroje
  • Acta Physica Polonica. A
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 120
http://linked.open...iv/tvurceVysledku
  • Chlup, Zdeněk
  • Dlouhý, Ivo
  • Havelcová, Martina
  • Sucharda, Zbyněk
  • Černý, Martin
  • Strachota, Adam
  • Kozák, Vladislav
  • Glogar, Petr
http://linked.open...ain/vavai/riv/wos
  • 000291836900026
http://linked.open...n/vavai/riv/zamer
issn
  • 0587-4246
number of pages
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