About: 2D Correlation Spectra Edited by the Sign of Relative Coupling Constant

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	Modifications (CSEc and CSEh) of recently published SQSQc and SQSQh pulse sequences are proposed and tested on detection of small (2 Hz) signed silicon carbon coupling constants. The new sequences increase signal intensity by simplifying the spectra. The signals are about four times stronger than in SQSQc or SQSQh spectra, achieving the sensitivity of E.COSY type experiment. The information about sign and magnitude of the coupling is preserved. CSEc and CSEh spectra for two silicon compounds are presented and compared. The two new sequences allow editing of heteronuclear correlation spectra according to the sign of the selected heteronuclear coupling constants. Modifications (CSEc and CSEh) of recently published SQSQc and SQSQh pulse sequences are proposed and tested on detection of small (2 Hz) signed silicon carbon coupling constants. The new sequences increase signal intensity by simplifying the spectra. The signals are about four times stronger than in SQSQc or SQSQh spectra, achieving the sensitivity of E.COSY type experiment. The information about sign and magnitude of the coupling is preserved. CSEc and CSEh spectra for two silicon compounds are presented and compared. The two new sequences allow editing of heteronuclear correlation spectra according to the sign of the selected heteronuclear coupling constants. (en)
Title	2D Correlation Spectra Edited by the Sign of Relative Coupling Constant 2D Correlation Spectra Edited by the Sign of Relative Coupling Constant (en)
skos:prefLabel	2D Correlation Spectra Edited by the Sign of Relative Coupling Constant 2D Correlation Spectra Edited by the Sign of Relative Coupling Constant (en)
skos:notation	RIV/67985858:_____/11:00357014!RIV12-AV0-67985858
http://linked.open...avai/riv/aktivita	P Z
http://linked.open...avai/riv/aktivity	P(IAA400720706), Z(AV0Z40720504)
http://linked.open...iv/cisloPeriodika	3
http://linked.open...vai/riv/dodaniDat	2012
http://linked.open...aciTvurceVysledku	Schraml, Jan Blechta, Vratislav
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Ústav chemických procesů AV ČR, v. v. i.
http://linked.open...dnocenehoVysledku	243989
http://linked.open...ai/riv/idVysledku	RIV/67985858:_____/11:00357014
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	nmr; nJ(Si,C); sign of coupling constant (en)
http://linked.open.../riv/klicoveSlovo	C) nJ(Si nmr sign of coupling constant
http://linked.open...odStatuVydavatele	GB - Spojené království Velké Británie a Severního Irska
http://linked.open...ontrolniKodProRIV	[087A0730F96E]
http://linked.open...i/riv/nazevZdroje	Magnetic Resonance in Chemistry
http://linked.open...in/vavai/riv/obor	CF
http://linked.open...ichTvurcuVysledku	2 (xsd:int)
http://linked.open...cetTvurcuVysledku	2 (xsd:int)
http://linked.open...vavai/riv/projekt	Structure of silyl moieties through J(29Si-13C) couplings as determined by triple {1H, 13C}29Si NMR experiments
http://linked.open...UplatneniVysledku	2011
http://linked.open...v/svazekPeriodika	49
http://linked.open...iv/tvurceVysledku	Schraml, Jan Blechta, Vratislav
http://linked.open...ain/vavai/riv/wos	000287890600003
http://linked.open...n/vavai/riv/zamer	Investigation of multiphase reacting systems for the design of processes important in synthesis and preparation of novel materials, in energy production and in environmental protection
issn	0749-1581
number of pages	6 (xsd:int)
http://bibframe.org/vocab/doi	10.1002/mrc.2720

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