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  • Crystallinity, purity and texture of TiO2 powder in dependence on the treatment mode (purification) of an amorphous reaction semi-product (titania organogel) was studied. Standard calcination was compared with various extraction techniques using fluids in sub/supercritical state. The suitable combination of extraction solvents and extraction conditions (temperature and pressure) was judged to synthesize TiO2 powders crystalline phase (Anatase) with a high specific surface area and purity. The optimal results were achieved by combined extraction procedures - subcritical water extraction and supercritical fluid extraction or pressurised liquid extraction. Moreover the possible tuning of the TiO2 powder pore-size distribution by regulation of temperature at constant pressure for the combination of subcritical water extraction and pressurised liquid extraction was found.
  • Crystallinity, purity and texture of TiO2 powder in dependence on the treatment mode (purification) of an amorphous reaction semi-product (titania organogel) was studied. Standard calcination was compared with various extraction techniques using fluids in sub/supercritical state. The suitable combination of extraction solvents and extraction conditions (temperature and pressure) was judged to synthesize TiO2 powders crystalline phase (Anatase) with a high specific surface area and purity. The optimal results were achieved by combined extraction procedures - subcritical water extraction and supercritical fluid extraction or pressurised liquid extraction. Moreover the possible tuning of the TiO2 powder pore-size distribution by regulation of temperature at constant pressure for the combination of subcritical water extraction and pressurised liquid extraction was found. (en)
Title
  • Super/Subcritical Fluid Extractions for Preparation of the Crystalline Titania
  • Super/Subcritical Fluid Extractions for Preparation of the Crystalline Titania (en)
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  • Super/Subcritical Fluid Extractions for Preparation of the Crystalline Titania
  • Super/Subcritical Fluid Extractions for Preparation of the Crystalline Titania (en)
skos:notation
  • RIV/67985858:_____/10:00341176!RIV11-GA0-67985858
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(GA104/09/0694), P(GP104/09/P290), Z(AV0Z40720504), Z(AV0Z50200510), Z(MSM0021620834)
http://linked.open...iv/cisloPeriodika
  • 2
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 291071
http://linked.open...ai/riv/idVysledku
  • RIV/67985858:_____/10:00341176
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • titania; supercritical fluid extraction; pressurised fluid extraction (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • NL - Nizozemsko
http://linked.open...ontrolniKodProRIV
  • [2FF150B00304]
http://linked.open...i/riv/nazevZdroje
  • Journal of Supercritical Fluids
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 52
http://linked.open...iv/tvurceVysledku
  • Benada, Oldřich
  • Cajthaml, Tomáš
  • Klusoň, Petr
  • Matějová, Lenka
  • Šolcová, Olga
  • Matěj, Z.
http://linked.open...ain/vavai/riv/wos
  • 000276115800007
http://linked.open...n/vavai/riv/zamer
issn
  • 0896-8446
number of pages
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