About: Synthesis and Properties of Mesoporous Silica-Alumina with Narrow Pore Size Distribution Obtained without Use of Pore-Regulating Agents     Goto   Sponge   NotDistinct   Permalink

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  • The synthesis of mesoporous silica-alumina (MSA) from Na metasilicate and AL nitrate without pore-regulating agents is described. The pore structure is almost exclusively formed by mesopores of diameters 3 - 5 nm. From X-Ray diffraction, electron microscopy and 27Al MAS NMR it follows that the MSA is amorphous with disordered pore arrangement, with majority of the Al atoms in octahedral coordination. The pore size distribution is much narrower in comparison to distributions of commercial silica-aluminas. The textural properties are influenced to only minor extent by treatments in water and calcination up to 800?C.
  • The synthesis of mesoporous silica-alumina (MSA) from Na metasilicate and AL nitrate without pore-regulating agents is described. The pore structure is almost exclusively formed by mesopores of diameters 3 - 5 nm. From X-Ray diffraction, electron microscopy and 27Al MAS NMR it follows that the MSA is amorphous with disordered pore arrangement, with majority of the Al atoms in octahedral coordination. The pore size distribution is much narrower in comparison to distributions of commercial silica-aluminas. The textural properties are influenced to only minor extent by treatments in water and calcination up to 800?C. (en)
  • Mezoporézní aluminosilikát MSA byl připraven z Na metasilikátu a dusičnanu hlinitého bez přídavku póry regulujících materiálů. Připravený monodisperzní materiál měl velmi úzkou distribuci pórů a vysoký specifický povrch. X-ray analýza potvrdila amorfnost materiálu s Al atomy v oktahedrální koordinaci. (cs)
Title
  • Synthesis and Properties of Mesoporous Silica-Alumina with Narrow Pore Size Distribution Obtained without Use of Pore-Regulating Agents
  • Synthesis and Properties of Mesoporous Silica-Alumina with Narrow Pore Size Distribution Obtained without Use of Pore-Regulating Agents (en)
  • Syntéza a vlastnosti mezoporézního aluminosilikátu s úzkou distribucí pórů (cs)
skos:prefLabel
  • Synthesis and Properties of Mesoporous Silica-Alumina with Narrow Pore Size Distribution Obtained without Use of Pore-Regulating Agents
  • Synthesis and Properties of Mesoporous Silica-Alumina with Narrow Pore Size Distribution Obtained without Use of Pore-Regulating Agents (en)
  • Syntéza a vlastnosti mezoporézního aluminosilikátu s úzkou distribucí pórů (cs)
skos:notation
  • RIV/67985858:_____/06:00055019!RIV07-AV0-67985858
http://linked.open.../vavai/riv/strany
  • 197;204
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(GA104/04/0963), P(GA104/06/0870), Z(AV0Z40720504)
http://linked.open...iv/cisloPeriodika
  • 1-3
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 502794
http://linked.open...ai/riv/idVysledku
  • RIV/67985858:_____/06:00055019
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • mesoporous silica-alumina; hydrothermal stability; pore size distribution (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • NL - Nizozemsko
http://linked.open...ontrolniKodProRIV
  • [21C7243451BB]
http://linked.open...i/riv/nazevZdroje
  • Microporous and Mesoporous Materials
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 96
http://linked.open...iv/tvurceVysledku
  • Šolcová, Olga
  • Vít, Zdeněk
http://linked.open...n/vavai/riv/zamer
issn
  • 1387-1811
number of pages
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