About: Simultaneous determination of metal traces by ICP-MS in environmental waters using SPE preconcentration on different polymeric sorbents

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About: Simultaneous determination of metal traces by ICP-MS in environmental waters using SPE preconcentration on different polymeric sorbents Goto Sponge NotDistinct Permalink

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	This paper deals with multielement profiling of microlements in the form of their isotopes Be-9, V-51, Co-59, Ni-60, Y-89, Cd-111, Pb-208, Th-232, and U-238. After their complexation by 4-(2-pyridylazo)resorcinol (PAR), 3,4-dihydroxy-9,10-dioxo-2-anthracenesulfonic acid sodium salt (ALS), 8-hydroxyquinoline-5-sulphonic acid (8-HQS), and ammonium pyrrolidinedithiocarbamate (APDC), the elements were preconcentrated and separated on Amberlite XAD-16 and Amberlite SDB-L prior to their analysis by inductively coupled plasma mass spectrometry. Various parameters such as pH, eluent type and volume, presence of surfactants and volume, and matrix effects on the retention of analytes were examined. Relative standard deviation and recovery values for four replicate determinations under optimal condition were in the range of 0.2-3.6 % and 59-98 %.The proposed method was applied to the determination of elements in lake water sample and industrial water. Recovery experiments with spiked water samples were performed. This paper deals with multielement profiling of microlements in the form of their isotopes Be-9, V-51, Co-59, Ni-60, Y-89, Cd-111, Pb-208, Th-232, and U-238. After their complexation by 4-(2-pyridylazo)resorcinol (PAR), 3,4-dihydroxy-9,10-dioxo-2-anthracenesulfonic acid sodium salt (ALS), 8-hydroxyquinoline-5-sulphonic acid (8-HQS), and ammonium pyrrolidinedithiocarbamate (APDC), the elements were preconcentrated and separated on Amberlite XAD-16 and Amberlite SDB-L prior to their analysis by inductively coupled plasma mass spectrometry. Various parameters such as pH, eluent type and volume, presence of surfactants and volume, and matrix effects on the retention of analytes were examined. Relative standard deviation and recovery values for four replicate determinations under optimal condition were in the range of 0.2-3.6 % and 59-98 %.The proposed method was applied to the determination of elements in lake water sample and industrial water. Recovery experiments with spiked water samples were performed. (en)
Title	Simultaneous determination of metal traces by ICP-MS in environmental waters using SPE preconcentration on different polymeric sorbents Simultaneous determination of metal traces by ICP-MS in environmental waters using SPE preconcentration on different polymeric sorbents (en)
skos:prefLabel	Simultaneous determination of metal traces by ICP-MS in environmental waters using SPE preconcentration on different polymeric sorbents Simultaneous determination of metal traces by ICP-MS in environmental waters using SPE preconcentration on different polymeric sorbents (en)
skos:notation	RIV/67179843:_____/12:00388775!RIV13-AV0-67179843
http://linked.open...avai/riv/aktivita	I P S
http://linked.open...avai/riv/aktivity	I, P(ED1.1.00/02.0073), S
http://linked.open...iv/cisloPeriodika	10
http://linked.open...vai/riv/dodaniDat	2013
http://linked.open...aciTvurceVysledku	Moos, Martin
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Centrum výzkumu globální změny AV ČR, v. v. i.
http://linked.open...dnocenehoVysledku	168106
http://linked.open...ai/riv/idVysledku	RIV/67179843:_____/12:00388775
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	solid phase extraction; Amberlite XAD-16; Amberlite SDB-L; ICP-MS; industrial waters; metal contaminants (en)
http://linked.open.../riv/klicoveSlovo	ICP-MS solid phase extraction Amberlite SDB-L Amberlite XAD-16 industrial waters metal contaminants
http://linked.open...odStatuVydavatele	SK - Slovenská republika
http://linked.open...ontrolniKodProRIV	[60ABEA7BA20A]
http://linked.open...i/riv/nazevZdroje	Chemical Papers
http://linked.open...in/vavai/riv/obor	EH
http://linked.open...ichTvurcuVysledku	1 (xsd:int)
http://linked.open...cetTvurcuVysledku	3 (xsd:int)
http://linked.open...vavai/riv/projekt	CzechGlobe - Center for Global Climate Change Impacts Studies
http://linked.open...UplatneniVysledku	2012
http://linked.open...v/svazekPeriodika	65
http://linked.open...iv/tvurceVysledku	Moos, Martin Holubova, Z. Sommer, L.
http://linked.open...ain/vavai/riv/wos	000306333200002
issn	0366-6352
number of pages	8 (xsd:int)
http://bibframe.org/vocab/doi	10.2478/s11696-012-0185-8

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