About: Characterization of 4,6-diazido-N-nitro-1,3,5-triazine-2-amine

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	4,6-Diazido-N-nitro-1,3,5-triazine-2-amine (DANT) was prepared with a 35% yield from cyanuric chloride in a three step process. DANT was characterized by IR and NMR spectroscopy (1H, 13C, 15N), single-crystal X-ray diffraction, and DTA. The crystal density of DANT is 1.849 gcm_3. The cyclization of one azido group and one nitrogen atom of the triazine group giving tetrazole was observed for DANT in a dimethyl sulfoxide solution using NMR spectroscopy. An equilibrium exists between the original DANT molecule and its cyclic form at a ratio of 7 : 3. The sensitivity of DANT to impact is between that for PETN and RDX, sensitivity to friction is between that for lead azide and PETN, and sensitivity to electric discharge is about the same as for PETN. DANT’s heat of combustion is 2060 kJmol_1. 4,6-Diazido-N-nitro-1,3,5-triazine-2-amine (DANT) was prepared with a 35% yield from cyanuric chloride in a three step process. DANT was characterized by IR and NMR spectroscopy (1H, 13C, 15N), single-crystal X-ray diffraction, and DTA. The crystal density of DANT is 1.849 gcm_3. The cyclization of one azido group and one nitrogen atom of the triazine group giving tetrazole was observed for DANT in a dimethyl sulfoxide solution using NMR spectroscopy. An equilibrium exists between the original DANT molecule and its cyclic form at a ratio of 7 : 3. The sensitivity of DANT to impact is between that for PETN and RDX, sensitivity to friction is between that for lead azide and PETN, and sensitivity to electric discharge is about the same as for PETN. DANT’s heat of combustion is 2060 kJmol_1. (en)
Title	Characterization of 4,6-diazido-N-nitro-1,3,5-triazine-2-amine Characterization of 4,6-diazido-N-nitro-1,3,5-triazine-2-amine (en)
skos:prefLabel	Characterization of 4,6-diazido-N-nitro-1,3,5-triazine-2-amine Characterization of 4,6-diazido-N-nitro-1,3,5-triazine-2-amine (en)
skos:notation	RIV/62690094:18470/12:50000943!RIV13-MSM-18470___
http://linked.open...avai/riv/aktivita	I Z
http://linked.open...avai/riv/aktivity	I, Z(MSM0021627501)
http://linked.open...iv/cisloPeriodika	3
http://linked.open...vai/riv/dodaniDat	2013
http://linked.open...aciTvurceVysledku	Lyčka, Antonín
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Univerzita Hradec Králové / Přírodovědecká fakulta
http://linked.open...dnocenehoVysledku	126854
http://linked.open...ai/riv/idVysledku	RIV/62690094:18470/12:50000943
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	X-ray diffraction; NMR spectroscopy; DANT; 4,6-Diazido-N-nitro-1,3,5-triazine-2-amine (en)
http://linked.open.../riv/klicoveSlovo	NMR spectroscopy X-ray diffraction 3 4 5-triazine-2-amine 6-Diazido-N-nitro-1 DANT
http://linked.open...odStatuVydavatele	DE - Spolková republika Německo
http://linked.open...ontrolniKodProRIV	[FD0B5C1D1283]
http://linked.open...i/riv/nazevZdroje	Propellants, explosives, pyrotechnics
http://linked.open...in/vavai/riv/obor	CC
http://linked.open...ichTvurcuVysledku	1 (xsd:int)
http://linked.open...cetTvurcuVysledku	4 (xsd:int)
http://linked.open...UplatneniVysledku	2012
http://linked.open...v/svazekPeriodika	37
http://linked.open...iv/tvurceVysledku	Růžička, Aleš Lyčka, Antonín Matyáš, Robert Musil, Tomáš
http://linked.open...ain/vavai/riv/wos	000305247000005
http://linked.open...n/vavai/riv/zamer	Aimed preparation of special compounds and materials and investigation of their physical and chemical properties and supramolecular structures
issn	0721-3115
number of pages	7 (xsd:int)
http://bibframe.org/vocab/doi	10.1002/prep.201000166
http://localhost/t...ganizacniJednotka	18470

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