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  • The existence of two new types of chloroderivates of cyclic acetone peroxides – 3-(chloromethyl)-3,6,6,9,9-pentamethyl-1,2,4,5,7,8-hexoxonane and 3,6-bis(chloromethyl)-3,6,9,9-tetramethyl-1,2,4,5,7,8-hexoxonane was proved by HPLC/MS/MS and NMR in the reaction products when acetone and hydrogen peroxide are mixed in the presence of excess hydrochloric acid (molar ratio hydrochloric acid to acetone nc/na=2.5). The details of analysis, and the conditions under which these asymmetric chloroderivates of cyclic peroxides form, are described.
  • The existence of two new types of chloroderivates of cyclic acetone peroxides – 3-(chloromethyl)-3,6,6,9,9-pentamethyl-1,2,4,5,7,8-hexoxonane and 3,6-bis(chloromethyl)-3,6,9,9-tetramethyl-1,2,4,5,7,8-hexoxonane was proved by HPLC/MS/MS and NMR in the reaction products when acetone and hydrogen peroxide are mixed in the presence of excess hydrochloric acid (molar ratio hydrochloric acid to acetone nc/na=2.5). The details of analysis, and the conditions under which these asymmetric chloroderivates of cyclic peroxides form, are described. (en)
Title
  • Study of TATP: Formation of new chloroderivates of triacetone triperoxide
  • Study of TATP: Formation of new chloroderivates of triacetone triperoxide (en)
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  • Study of TATP: Formation of new chloroderivates of triacetone triperoxide
  • Study of TATP: Formation of new chloroderivates of triacetone triperoxide (en)
skos:notation
  • RIV/62690094:18470/11:43866582!RIV12-MSM-18470___
http://linked.open...avai/riv/aktivita
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  • V, Z(MSM0021627501)
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  • 3
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  • 233129
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  • RIV/62690094:18470/11:43866582
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  • TATP; NMR; mass spectrometry; 3,3,6,6,9,9-hexamethyl-1,2,4,5,7,8-hexoxonane; 3,6-bis(chloromethyl)-3,6,9,9-tetramethyl-1,2,4,5,7,8-hexoxonane; 3-(chloromethyl)-3,6,6,9,9-pentamethyl-1,2,4,5,7,8-hexoxonane (en)
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  • DE - Spolková republika Německo
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  • [3EFD332857A2]
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  • Propellants, explosives, pyrotechnics
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  • 36
http://linked.open...iv/tvurceVysledku
  • Lyčka, Antonín
http://linked.open...ain/vavai/riv/wos
  • 000292407600003
http://linked.open...n/vavai/riv/zamer
issn
  • 0721-3115
number of pages
http://bibframe.org/vocab/doi
  • 10.1002/prep.201000158
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  • 18470
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