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  • The present study deals with the determination of residues of selected antibiotics from the group of sulfonamides in water ecosystem. The target analytes included ten sulfonamides: sulfaguanidine, sulfadiazine, sulfathiazole, sulfapyridine, sulfamerazine, sulfadimidine, sulfamethoxazole, sulfadoxine, sulfaclozine and sulfadimethoxine. The optimized methods should be applied for the matrices as surface or waste water and bottom river sediment. The attention was first focused on optimization of the method for identification and quantification of selected sulfonamides using high-performance liquid chromatography coupled with diode array detector (HPLC/DAD). The methods of solid phase extraction (SPE) and pressurized solvent extraction (PSE) were optimized for extraction, pre-concentration and purification of the matrices.
  • The present study deals with the determination of residues of selected antibiotics from the group of sulfonamides in water ecosystem. The target analytes included ten sulfonamides: sulfaguanidine, sulfadiazine, sulfathiazole, sulfapyridine, sulfamerazine, sulfadimidine, sulfamethoxazole, sulfadoxine, sulfaclozine and sulfadimethoxine. The optimized methods should be applied for the matrices as surface or waste water and bottom river sediment. The attention was first focused on optimization of the method for identification and quantification of selected sulfonamides using high-performance liquid chromatography coupled with diode array detector (HPLC/DAD). The methods of solid phase extraction (SPE) and pressurized solvent extraction (PSE) were optimized for extraction, pre-concentration and purification of the matrices. (en)
Title
  • Optimization of analytical methods for the determination of residues of selected pharmaceuticals in the aquatic environment
  • Optimization of analytical methods for the determination of residues of selected pharmaceuticals in the aquatic environment (en)
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  • Optimization of analytical methods for the determination of residues of selected pharmaceuticals in the aquatic environment
  • Optimization of analytical methods for the determination of residues of selected pharmaceuticals in the aquatic environment (en)
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  • RIV/62157124:16270/14:43872722!RIV15-MSM-16270___
http://linked.open...avai/riv/aktivita
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  • S
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  • 34941
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  • RIV/62157124:16270/14:43872722
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  • pressurized solvent extraction (PSE); solid phase extraction (SPE); HPLC/DAD; sulfonamides (en)
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  • [92224ADAD09B]
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  • Brno
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  • Brno
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  • CECE 2014: 11th International Interdisciplinary Meeting on Bioanalysis
http://linked.open...in/vavai/riv/obor
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  • Vávrová, Milada
  • Járová, Kateřina
  • Oborná, Jana
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http://linked.open.../riv/zahajeniAkce
number of pages
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  • Institute of Analytical Chemistry AS CR, v. v. i.,
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  • 978-80-904959-2-0
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  • 16270
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