About: Optimization of the HS-SPME method coupled with GC/?ECD for determination of methylmercury in water

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About: Optimization of the HS-SPME method coupled with GC/?ECD for determination of methylmercury in water Goto Sponge NotDistinct Permalink

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	The aim of this study was the optimization of the Solid Phase Micro-extraction (SPME) method and the optimization of gas chromatography using an electron capture detector method. %22Head-space%22 (HS-SPME) is used for the extraction of volatile compounds from a sample. In our case, the sample matrix was water. The analytical procedure involves derivatization of ionic mercury with sodium tetraethylborate in a sample vial and following extraction with a silica polydimethylsiloxane coated fibre. Standard methylmercury was used for the optimization of the SPME method. The fibre, extraction time, temperature and pH, were optimized for the extraction method by HS-SPME. The aim of this study was the optimization of the Solid Phase Micro-extraction (SPME) method and the optimization of gas chromatography using an electron capture detector method. %22Head-space%22 (HS-SPME) is used for the extraction of volatile compounds from a sample. In our case, the sample matrix was water. The analytical procedure involves derivatization of ionic mercury with sodium tetraethylborate in a sample vial and following extraction with a silica polydimethylsiloxane coated fibre. Standard methylmercury was used for the optimization of the SPME method. The fibre, extraction time, temperature and pH, were optimized for the extraction method by HS-SPME. (en)
Title	Optimization of the HS-SPME method coupled with GC/?ECD for determination of methylmercury in water Optimization of the HS-SPME method coupled with GC/?ECD for determination of methylmercury in water (en)
skos:prefLabel	Optimization of the HS-SPME method coupled with GC/?ECD for determination of methylmercury in water Optimization of the HS-SPME method coupled with GC/?ECD for determination of methylmercury in water (en)
skos:notation	RIV/62157124:16270/14:43872720!RIV15-MSM-16270___
http://linked.open...avai/riv/aktivita	S Z
http://linked.open...avai/riv/aktivity	S, Z(MSM6215712402)
http://linked.open...iv/cisloPeriodika	12B
http://linked.open...vai/riv/dodaniDat	2015
http://linked.open...aciTvurceVysledku	Králová, Zuzana Šucman, Emanuel Komárková, Petra
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Veterinární a farmaceutická univerzita Brno / Fakulta veterinární hygieny a ekologie
http://linked.open...dnocenehoVysledku	34986
http://linked.open...ai/riv/idVysledku	RIV/62157124:16270/14:43872720
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	gas chromatography; optimization; solid phase micro-extraction; methylmercury (en)
http://linked.open.../riv/klicoveSlovo	methylmercury gas chromatography optimization solid phase micro-extraction
http://linked.open...odStatuVydavatele	DE - Spolková republika Německo
http://linked.open...ontrolniKodProRIV	[4C8D9941D268]
http://linked.open...i/riv/nazevZdroje	Fresenius Environmental Bulletin
http://linked.open...in/vavai/riv/obor	DN
http://linked.open...ichTvurcuVysledku	3 (xsd:int)
http://linked.open...cetTvurcuVysledku	4 (xsd:int)
http://linked.open...UplatneniVysledku	2014
http://linked.open...v/svazekPeriodika	23
http://linked.open...iv/tvurceVysledku	Vávrová, Milada Králová, Zuzana Šucman, Emanuel Komárková, Petra
http://linked.open...ain/vavai/riv/wos	000348744900015
http://linked.open...n/vavai/riv/zamer	Veterinary aspects of food safety and quality
issn	1018-4619
number of pages	4 (xsd:int)
http://localhost/t...ganizacniJednotka	16270

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