About: Chromatographic Method of Determination of Biogenic Amines in Meat Products During Fermentation and Long-term Storage (in Czech).     Goto   Sponge   NotDistinct   Permalink

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  • Liquid chromatographic procedures employing two derivatisation reagents dansylchloride and phthalaldehyde (OPA) were compared and applied for the determination of biogenic amines in meat products during fermentation and long term storage. Both methods give the similar results in terms of limits of detection, repeatability, recovery and accuracy. Secondary amines (spermine and spermidine) do not react with phthalaldehyde thus their LC determination after derivatization with dansylchloride is only possible. The content of secondary amines during fermentation and/or long term storage is nearly constant or slightly decreases, thus their determination in both cases is not necessarry. Liqiud chromatographic procedure emloying derivatization with phthalaldehyde (OPA) is faster, much simpler in term of pretreatment of samples and it can be fully automated using an inteligent autosampler.
  • Liquid chromatographic procedures employing two derivatisation reagents dansylchloride and phthalaldehyde (OPA) were compared and applied for the determination of biogenic amines in meat products during fermentation and long term storage. Both methods give the similar results in terms of limits of detection, repeatability, recovery and accuracy. Secondary amines (spermine and spermidine) do not react with phthalaldehyde thus their LC determination after derivatization with dansylchloride is only possible. The content of secondary amines during fermentation and/or long term storage is nearly constant or slightly decreases, thus their determination in both cases is not necessarry. Liqiud chromatographic procedure emloying derivatization with phthalaldehyde (OPA) is faster, much simpler in term of pretreatment of samples and it can be fully automated using an inteligent autosampler. (en)
  • Liquid chromatographic procedures employing two derivatisation reagents dansylchloride and phthalaldehyde (OPA) were compared and applied for the determination of biogenic amines in meat products during fermentation and long term storage. Both methods give the similar results in terms of limits of detection, repeatability, recovery and accuracy. Secondary amines (spermine and spermidine) do not react with phthalaldehyde thus their LC determination after derivatization with dansylchloride is only possible. The content of secondary amines during fermentation and/or long term storage is nearly constant or slightly decreases, thus their determination in both cases is not necessarry. Liqiud chromatographic procedure emloying derivatization with phthalaldehyde (OPA) is faster, much simpler in term of pretreatment of samples and it can be fully automated using an inteligent autosampler. (cs)
Title
  • Chromatographic Method of Determination of Biogenic Amines in Meat Products During Fermentation and Long-term Storage (in Czech). (en)
  • Chromatografické metody stanovení biogenních aminů v masných výrobcích během fermentace a dlouhodobého skladování
  • Chromatografické metody stanovení biogenních aminů v masných výrobcích během fermentace a dlouhodobého skladování (cs)
skos:prefLabel
  • Chromatographic Method of Determination of Biogenic Amines in Meat Products During Fermentation and Long-term Storage (in Czech). (en)
  • Chromatografické metody stanovení biogenních aminů v masných výrobcích během fermentace a dlouhodobého skladování
  • Chromatografické metody stanovení biogenních aminů v masných výrobcích během fermentace a dlouhodobého skladování (cs)
skos:notation
  • RIV/62156489:43210/04:00000832!RIV/2005/MSM/432105/N
http://linked.open.../vavai/riv/strany
  • 432;437
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(MSM 432100001)
http://linked.open...iv/cisloPeriodika
  • 4
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 557714
http://linked.open...ai/riv/idVysledku
  • RIV/62156489:43210/04:00000832
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • biogenic amines;chromatography;meat products (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • CZ - Česká republika
http://linked.open...ontrolniKodProRIV
  • [04EEBBF7718B]
http://linked.open...i/riv/nazevZdroje
  • Chemické listy
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 98
http://linked.open...iv/tvurceVysledku
  • Kubáň, Vlastimil
  • Klejdus, Bořivoj
  • Komprda, Tomáš
  • Smělá, Dana
http://linked.open...n/vavai/riv/zamer
issn
  • 0009-2770
number of pages
http://localhost/t...ganizacniJednotka
  • 43210
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