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  • Setup of Mossbauer spectrometers (MS) for structural, phase, and magnetic characterization of iron-or tin-containing samples is presented. This comprehensive line of Fe-57 and Sn-119 Mossbauer spectrometers covers transmission spectrometers (TMS) for room-temperature (RT) measurements, temperature dependent measurements and measurements in an external magnetic field. An RT Conversion Electron/Conversion X-ray Mossbauer technique (CEMS/CXMS) is also available. The main concept of the RT MS is a table-top spectrometric bench with a control unit based on special-purpose hardware or standard PC platform. The first way offers a compact design and PC independent spectra collection system. The second setup, a PC-based system, which uses commercial devices and LabVIEW software, offers easy customization and enables advancement in spectrometer construction. The both types of control systems are able to operate special parts (velocity transducers, gamma-ray detectors) of unusual spectrometric benches. The standard velocity axis range is up to +/- 20 mm/s with a maximum nonlinearity of 0.1%. Applicable measuring conditions of presented TMSs cover a cryogenic temperature range from 1.5 up to 300 K and high temperature range from RT up to 1000 degrees C. With in-field low-temperature MS, we are able to analyze samples normally in the external magnetic fields up to 8 T (in temperature interval from 1.5 up to 300 K). In addition, special modes of measurements can be applied including backscattering gamma-ray geometry or measurement in an inert or controlled-humidity atmosphere. Technical details and construction aspects of spectrometers are presented.
  • Setup of Mossbauer spectrometers (MS) for structural, phase, and magnetic characterization of iron-or tin-containing samples is presented. This comprehensive line of Fe-57 and Sn-119 Mossbauer spectrometers covers transmission spectrometers (TMS) for room-temperature (RT) measurements, temperature dependent measurements and measurements in an external magnetic field. An RT Conversion Electron/Conversion X-ray Mossbauer technique (CEMS/CXMS) is also available. The main concept of the RT MS is a table-top spectrometric bench with a control unit based on special-purpose hardware or standard PC platform. The first way offers a compact design and PC independent spectra collection system. The second setup, a PC-based system, which uses commercial devices and LabVIEW software, offers easy customization and enables advancement in spectrometer construction. The both types of control systems are able to operate special parts (velocity transducers, gamma-ray detectors) of unusual spectrometric benches. The standard velocity axis range is up to +/- 20 mm/s with a maximum nonlinearity of 0.1%. Applicable measuring conditions of presented TMSs cover a cryogenic temperature range from 1.5 up to 300 K and high temperature range from RT up to 1000 degrees C. With in-field low-temperature MS, we are able to analyze samples normally in the external magnetic fields up to 8 T (in temperature interval from 1.5 up to 300 K). In addition, special modes of measurements can be applied including backscattering gamma-ray geometry or measurement in an inert or controlled-humidity atmosphere. Technical details and construction aspects of spectrometers are presented. (en)
Title
  • Setup of Mossbauer Spectrometers at RCPTM
  • Setup of Mossbauer Spectrometers at RCPTM (en)
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  • Setup of Mossbauer Spectrometers at RCPTM
  • Setup of Mossbauer Spectrometers at RCPTM (en)
skos:notation
  • RIV/61989592:15310/12:33140944!RIV13-MSM-15310___
http://linked.open...avai/riv/aktivita
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  • P(ED2.1.00/03.0058)
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http://linked.open...aciTvurceVysledku
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  • 167618
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  • RIV/61989592:15310/12:33140944
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  • Mossbauer spectrometer; Mossbauer spectroscopy (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...ontrolniKodProRIV
  • [D47DF3BF68A9]
http://linked.open...v/mistoKonaniAkce
  • Olomouc
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  • New York
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  • AIP Conference Proceedings
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  • Jančík, Dalibor
  • Novák, Petr
  • Pechoušek, Jiří
  • Frydrych, Jiří
  • Navařík, Jakub
http://linked.open...vavai/riv/typAkce
http://linked.open...ain/vavai/riv/wos
  • 000311909900023
http://linked.open.../riv/zahajeniAkce
issn
  • 0094-243X
number of pages
http://bibframe.org/vocab/doi
  • 10.1063/1.4759489
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  • American Institute of Physics
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  • 978-0-7354-1101-2
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  • 15310
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