About: Synthesis, characterization and in vitro cytotoxicity of the first palladium(II) oxalato complexes involving adenine based ligands     Goto   Sponge   NotDistinct   Permalink

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  • The first [Pd(Ln)2(ox)] . xH2O oxalato (ox) complexes involving 2 chloro-N6-(benzyl)-9-isopropyladenine (L1; complex 1), 2 chloro-N6-(4-methoxybenzyl)-9-isopropyladenine (L2; 2), 2 chloro-N6-(2,3-dimethoxybenzyl)-9-isopropyladenine (L3; 3), 2 chloro-N6-(2,4-dimethoxybenzyl)-9-isopropyladenine (L4; 4), and 2 chloro-N6-(4-methylbenzyl)-9-isopropyladenine (L5; 5) have been synthesized by the reactions of potassium bis(oxalato)palladate(II) dihydrate, [K2Pd(ox)2].2H2O, with the mentioned organic compounds (H2ox = oxalic acid; x = 0 for 1-3 and 5 or 2 for 4). Elemental analyses (C, H, N), FTIR, Raman and NMR (1H, 13C, 15N) spectroscopies, conductivity measurements and thermal studies (thermogravimetric and differential thermal analysis, TG/DTA) have been used to characterize the prepared complexes. The molecular structures of [Pd(L2)2(ox)] (2) and [Pd(L5)2(ox)] . L5 . Me2CO (5 . L5 . Me2CO) have been determined by a single crystal X ray analysis. The geometry of these complexes is slightly distorted square
  • The first [Pd(Ln)2(ox)] . xH2O oxalato (ox) complexes involving 2 chloro-N6-(benzyl)-9-isopropyladenine (L1; complex 1), 2 chloro-N6-(4-methoxybenzyl)-9-isopropyladenine (L2; 2), 2 chloro-N6-(2,3-dimethoxybenzyl)-9-isopropyladenine (L3; 3), 2 chloro-N6-(2,4-dimethoxybenzyl)-9-isopropyladenine (L4; 4), and 2 chloro-N6-(4-methylbenzyl)-9-isopropyladenine (L5; 5) have been synthesized by the reactions of potassium bis(oxalato)palladate(II) dihydrate, [K2Pd(ox)2].2H2O, with the mentioned organic compounds (H2ox = oxalic acid; x = 0 for 1-3 and 5 or 2 for 4). Elemental analyses (C, H, N), FTIR, Raman and NMR (1H, 13C, 15N) spectroscopies, conductivity measurements and thermal studies (thermogravimetric and differential thermal analysis, TG/DTA) have been used to characterize the prepared complexes. The molecular structures of [Pd(L2)2(ox)] (2) and [Pd(L5)2(ox)] . L5 . Me2CO (5 . L5 . Me2CO) have been determined by a single crystal X ray analysis. The geometry of these complexes is slightly distorted square (en)
Title
  • Synthesis, characterization and in vitro cytotoxicity of the first palladium(II) oxalato complexes involving adenine based ligands
  • Synthesis, characterization and in vitro cytotoxicity of the first palladium(II) oxalato complexes involving adenine based ligands (en)
skos:prefLabel
  • Synthesis, characterization and in vitro cytotoxicity of the first palladium(II) oxalato complexes involving adenine based ligands
  • Synthesis, characterization and in vitro cytotoxicity of the first palladium(II) oxalato complexes involving adenine based ligands (en)
skos:notation
  • RIV/61989592:15310/09:00010068!RIV10-MSM-15310___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(MSM6198959218)
http://linked.open...iv/cisloPeriodika
  • 7
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 345086
http://linked.open...ai/riv/idVysledku
  • RIV/61989592:15310/09:00010068
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • Palladium(II) complexes; Oxalate; Adenine derivatives; In vitro cytotoxicity; X ray structure (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • US - Spojené státy americké
http://linked.open...ontrolniKodProRIV
  • [EE4A1E708230]
http://linked.open...i/riv/nazevZdroje
  • Journal of Inorganic Biochemistry
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 103
http://linked.open...iv/tvurceVysledku
  • Trávníček, Zdeněk
  • Štarha, Pavel
  • Popa, Igor
http://linked.open...n/vavai/riv/zamer
issn
  • 0162-0134
number of pages
http://localhost/t...ganizacniJednotka
  • 15310
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