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Description
  • Obsahem článku je derivatizace kyseliny orotické do různých forem a jejich vyhodnocení pomocí GC/MS. (cs)
  • Derivatization of orotic acid (OA) into various forms (trimethylsilylderivate, alkyl ester and per-methylated derivate) and their evaluation by GC/MS is described. The tested approach includes ion-exchange SPE clean-up, evaporation and chemical reaction with different types of derivatization agents (N,O-bis-(trimethylsilyl)trifluoroacetamide with trimethylchlorosilane, butanol with acetylchloride and ethereal solution of diazomethane).
  • Derivatization of orotic acid (OA) into various forms (trimethylsilylderivate, alkyl ester and per-methylated derivate) and their evaluation by GC/MS is described. The tested approach includes ion-exchange SPE clean-up, evaporation and chemical reaction with different types of derivatization agents (N,O-bis-(trimethylsilyl)trifluoroacetamide with trimethylchlorosilane, butanol with acetylchloride and ethereal solution of diazomethane). (en)
Title
  • Analytical derivatization - a tool for determination of orotic acid
  • Analytical derivatization - a tool for determination of orotic acid (en)
  • Analytická derivatizace - prostředek ke stanovení koncentrace kyseliny orotové (cs)
skos:prefLabel
  • Analytical derivatization - a tool for determination of orotic acid
  • Analytical derivatization - a tool for determination of orotic acid (en)
  • Analytická derivatizace - prostředek ke stanovení koncentrace kyseliny orotové (cs)
skos:notation
  • RIV/61989592:15110/04:00001902!RIV06-GA0-15110___
http://linked.open.../vavai/riv/strany
  • 303-309
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(GP303/02/D010), Z(MSM 153100013)
http://linked.open...iv/cisloPeriodika
  • 2
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 554330
http://linked.open...ai/riv/idVysledku
  • RIV/61989592:15110/04:00001902
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • derivatization; GC; orotic acid (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • NL - Nizozemsko
http://linked.open...ontrolniKodProRIV
  • [280FADC48257]
http://linked.open...i/riv/nazevZdroje
  • Journal of Chromatography. B, Analytical Technologies in the Biomedical and Life Sciences
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 799
http://linked.open...iv/tvurceVysledku
  • Barták, Petr
  • Adam, Tomáš
  • Čáp, Lubomír
  • Friedecký, David
  • Hušková, R.
http://linked.open...n/vavai/riv/zamer
issn
  • 1570-0232
number of pages
http://localhost/t...ganizacniJednotka
  • 15110
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