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| rdf:type
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| Description
| - Differential thermal analysis (DTA) and Differential Scanning Calorimetry (DSC) are two of the methods that are suitable for obtaining thermo-physical and thermo-dynamical data. This paper deals with the influence of the experimental conditions settings of the used DTA and DSC methods in relation to the obtained data. The paper is focused on the study of heating/cooling rate and mass influence of the sample on shifting of the phase transformations temperatures and size of the thermal effects of alpha-gamma, gamma-delta phase transformations and melting of “pure Fe”. Sample mass and heating/cooling rate belong to the frequently and easily changing parameters and their influence on the obtained data is substantial. The study was aimed both at low temperature and high temperature regions. DTA measurements were realised using the Setaram Setsys 18TM laboratory system, and DSC measurements using the Setaram MHTC laboratory system. The samples of “pure Fe” (with different mass) were analysed at several controlled heating/cooling rates. On the basis of adjusted experimental conditions (different heating/cooling rates and different masses of samples), the experimental data set was obtained and corresponding dependences were derived. Using the corresponding dependences the corrections can be applied to minimise the influence of experimental conditions on studied data for investigated alloys (samples). Application of derived dependences can substantially contribute to lowering (minimising) of the experimental conditions influence and enables an extrapolation to the so called “zero” mass and “zero” heating rate.
- Differential thermal analysis (DTA) and Differential Scanning Calorimetry (DSC) are two of the methods that are suitable for obtaining thermo-physical and thermo-dynamical data. This paper deals with the influence of the experimental conditions settings of the used DTA and DSC methods in relation to the obtained data. The paper is focused on the study of heating/cooling rate and mass influence of the sample on shifting of the phase transformations temperatures and size of the thermal effects of alpha-gamma, gamma-delta phase transformations and melting of “pure Fe”. Sample mass and heating/cooling rate belong to the frequently and easily changing parameters and their influence on the obtained data is substantial. The study was aimed both at low temperature and high temperature regions. DTA measurements were realised using the Setaram Setsys 18TM laboratory system, and DSC measurements using the Setaram MHTC laboratory system. The samples of “pure Fe” (with different mass) were analysed at several controlled heating/cooling rates. On the basis of adjusted experimental conditions (different heating/cooling rates and different masses of samples), the experimental data set was obtained and corresponding dependences were derived. Using the corresponding dependences the corrections can be applied to minimise the influence of experimental conditions on studied data for investigated alloys (samples). Application of derived dependences can substantially contribute to lowering (minimising) of the experimental conditions influence and enables an extrapolation to the so called “zero” mass and “zero” heating rate. (en)
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| Title
| - Influence of experimental conditions on data obtained by thermal analysis methods
- Influence of experimental conditions on data obtained by thermal analysis methods (en)
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| skos:prefLabel
| - Influence of experimental conditions on data obtained by thermal analysis methods
- Influence of experimental conditions on data obtained by thermal analysis methods (en)
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| skos:notation
| - RIV/61989100:27360/13:86087826!RIV14-TA0-27360___
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| http://linked.open...avai/riv/aktivita
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| http://linked.open...avai/riv/aktivity
| - P(ED0040/01/01), P(GAP107/11/1566), P(TA03011277)
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| http://linked.open...vai/riv/dodaniDat
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| http://linked.open...aciTvurceVysledku
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| http://linked.open.../riv/druhVysledku
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| http://linked.open...iv/duvernostUdaju
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| http://linked.open...titaPredkladatele
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| http://linked.open...dnocenehoVysledku
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| http://linked.open...ai/riv/idVysledku
| - RIV/61989100:27360/13:86087826
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| http://linked.open...riv/jazykVysledku
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| http://linked.open.../riv/klicovaSlova
| - sample mass; heating/cooling rate; experimental conditions; DSC; DTA (en)
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| http://linked.open.../riv/klicoveSlovo
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| http://linked.open...ontrolniKodProRIV
| |
| http://linked.open...v/mistoKonaniAkce
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| http://linked.open...i/riv/mistoVydani
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| http://linked.open...i/riv/nazevZdroje
| - METAL 2013 : 22nd International Conference on Metallurgy and Materials : conference proceedings : May 15th - 17th 2013, Hotel Voronez I, Brno Czech Republic, EU [CD-ROM]
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| http://linked.open...in/vavai/riv/obor
| |
| http://linked.open...ichTvurcuVysledku
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| http://linked.open...cetTvurcuVysledku
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| http://linked.open...vavai/riv/projekt
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| http://linked.open...UplatneniVysledku
| |
| http://linked.open...iv/tvurceVysledku
| - Dobrovská, Jana
- Petlák, Daniel
- Smetana, Bedřich
- Szurman, Ivo
- Zlá, Simona
- Žaludová, Monika
- Rosypalová, Silvie
- Štvrtňová, Alice
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| http://linked.open...vavai/riv/typAkce
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| http://linked.open.../riv/zahajeniAkce
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| number of pages
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| http://purl.org/ne...btex#hasPublisher
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| https://schema.org/isbn
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| http://localhost/t...ganizacniJednotka
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