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  • The paper deals with the study possibilities of heat capacities, mainly of metallic systems (alloys) on the basis of Fe (Fe-C). Possibilities of theoretical calculations dependencies of heat capacities on temperature are presented in this work in a wide temperature region. Theoretical basis of heat capacities determination using Neumann-Kopp rule is discussed. Experimental possibilities of heat capacities acquisition are determined by our experimental base. Two classical thermal analysers (2D DSC sensors) are used at our working site: Setaram SETSYS 18TM and Netzsch STA 449 F3 Jupiter. The third experimental system is Setaram MHTC (Multi High Temperature Calorimeter). MHTC is equipped with unique 3D DSC sensors. Furthermore, the MHTC enables to analyse samples with substantially higher sample weight (2.5; up to 30 g respectively). It should be possible to obtain more accurate results with MHTC in comparison with classical 2D DSC sensors (max. sample weight approximately 500 mg). Various methods of heat capacities measurement and calculations are presented in the paper (continuous, stepped and DROP method, theoretical Neumann-Kopp rule). Initial results obtained at our working site are presented in this paper.
  • The paper deals with the study possibilities of heat capacities, mainly of metallic systems (alloys) on the basis of Fe (Fe-C). Possibilities of theoretical calculations dependencies of heat capacities on temperature are presented in this work in a wide temperature region. Theoretical basis of heat capacities determination using Neumann-Kopp rule is discussed. Experimental possibilities of heat capacities acquisition are determined by our experimental base. Two classical thermal analysers (2D DSC sensors) are used at our working site: Setaram SETSYS 18TM and Netzsch STA 449 F3 Jupiter. The third experimental system is Setaram MHTC (Multi High Temperature Calorimeter). MHTC is equipped with unique 3D DSC sensors. Furthermore, the MHTC enables to analyse samples with substantially higher sample weight (2.5; up to 30 g respectively). It should be possible to obtain more accurate results with MHTC in comparison with classical 2D DSC sensors (max. sample weight approximately 500 mg). Various methods of heat capacities measurement and calculations are presented in the paper (continuous, stepped and DROP method, theoretical Neumann-Kopp rule). Initial results obtained at our working site are presented in this paper. (en)
Title
  • Possibilities of heat capacity measurement of metallic systems
  • Possibilities of heat capacity measurement of metallic systems (en)
skos:prefLabel
  • Possibilities of heat capacity measurement of metallic systems
  • Possibilities of heat capacity measurement of metallic systems (en)
skos:notation
  • RIV/61989100:27360/12:86083394!RIV13-GA0-27360___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(ED0040/01/01), P(FR-TI3/077), P(GAP107/11/1566)
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 160059
http://linked.open...ai/riv/idVysledku
  • RIV/61989100:27360/12:86083394
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • DROP; hf-DSC; DSC; metallic systems; thermal analysis; Heat capacity (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...ontrolniKodProRIV
  • [FE0ECBD5B911]
http://linked.open...v/mistoKonaniAkce
  • Brno
http://linked.open...i/riv/mistoVydani
  • Ostrava
http://linked.open...i/riv/nazevZdroje
  • METAL 2012 : 21st International Conference on Metallurgy and Materials : conference proceedings
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...iv/tvurceVysledku
  • Dobrovská, Jana
  • Klus, Petr
  • Smetana, Bedřich
  • Tkadlečková, Markéta
  • Zlá, Simona
  • Žaludová, Monika
  • Rosypalová, Silvie
http://linked.open...vavai/riv/typAkce
http://linked.open.../riv/zahajeniAkce
number of pages
http://purl.org/ne...btex#hasPublisher
  • Tanger s.r.o.
https://schema.org/isbn
  • 978-80-87294-31-4
http://localhost/t...ganizacniJednotka
  • 27360
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