About: Monodisperse superparamagnetic nanoparticles by thermolysis of Fe(III) oleate and mandelate complexes

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About: Monodisperse superparamagnetic nanoparticles by thermolysis of Fe(III) oleate and mandelate complexes Goto Sponge NotDistinct Permalink

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	Monodisperse superparamagnetic iron oxide nanoparticles of controlled size were synthesized by thermal decomposition of organic iron compounds in different high-boiling solvents in the presence of oleic acid and/or oleylamine. The compounds included Fe(III) oleate and mandelate, formed from FeCl3 and the respective acids. The size of the nanoparticles was easily tuned to 8–27 nm by varying the experimental conditions. The nanoparticles were characterized using X-ray diffraction (XRD), transmission electron microscopy (TEM), and magnetization measurements. The hydrophobic coating of the particles was analyzed by thermogravimetric analysis (TGA) and atomic absorption spectroscopy (AAS). To make the particles biocompatible and water dispersible, nontoxic hydrophilic poly(ethylene glycol) derivatives were synthesized and used for phase transfer of hydrophobic particles into water using a ligand-exchange procedure. Monodisperse superparamagnetic iron oxide nanoparticles of controlled size were synthesized by thermal decomposition of organic iron compounds in different high-boiling solvents in the presence of oleic acid and/or oleylamine. The compounds included Fe(III) oleate and mandelate, formed from FeCl3 and the respective acids. The size of the nanoparticles was easily tuned to 8–27 nm by varying the experimental conditions. The nanoparticles were characterized using X-ray diffraction (XRD), transmission electron microscopy (TEM), and magnetization measurements. The hydrophobic coating of the particles was analyzed by thermogravimetric analysis (TGA) and atomic absorption spectroscopy (AAS). To make the particles biocompatible and water dispersible, nontoxic hydrophilic poly(ethylene glycol) derivatives were synthesized and used for phase transfer of hydrophobic particles into water using a ligand-exchange procedure. (en)
Title	Monodisperse superparamagnetic nanoparticles by thermolysis of Fe(III) oleate and mandelate complexes Monodisperse superparamagnetic nanoparticles by thermolysis of Fe(III) oleate and mandelate complexes (en)
skos:prefLabel	Monodisperse superparamagnetic nanoparticles by thermolysis of Fe(III) oleate and mandelate complexes Monodisperse superparamagnetic nanoparticles by thermolysis of Fe(III) oleate and mandelate complexes (en)
skos:notation	RIV/61389013:_____/14:00431295!RIV15-GA0-61389013
http://linked.open...avai/riv/aktivita	I P
http://linked.open...avai/riv/aktivity	I, P(7E12053), P(GAP206/12/0381)
http://linked.open...iv/cisloPeriodika	9
http://linked.open...vai/riv/dodaniDat	2015
http://linked.open...aciTvurceVysledku	Kovářová, Jana Horák, Daniel Konefal, Rafal Patsula, Vitalii
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Ústav makromolekulární chemie AV ČR, v. v. i.
http://linked.open...dnocenehoVysledku	30462
http://linked.open...ai/riv/idVysledku	RIV/61389013:_____/14:00431295
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	superparamagnetic; nanoparticles; iron oxide (en)
http://linked.open.../riv/klicoveSlovo	iron oxide superparamagnetic nanoparticles
http://linked.open...odStatuVydavatele	DE - Spolková republika Německo
http://linked.open...ontrolniKodProRIV	[C1EB50F1AA62]
http://linked.open...i/riv/nazevZdroje	Colloid and Polymer Science
http://linked.open...in/vavai/riv/obor	CD
http://linked.open...ichTvurcuVysledku	4 (xsd:int)
http://linked.open...cetTvurcuVysledku	5 (xsd:int)
http://linked.open...vavai/riv/projekt	Development of ultrasensitive electrochemical immunosensors for early detection of clinically significant biomarkers of malignant diseases Nanosystems for early Diagnosis of Neurodegenerative Diseases
http://linked.open...UplatneniVysledku	2014
http://linked.open...v/svazekPeriodika	292
http://linked.open...iv/tvurceVysledku	Horák, Daniel Kovářová, Jana Petrovský, Eduard Konefal, Rafal Patsula, Vitalii
http://linked.open...ain/vavai/riv/wos	000341489900006
issn	0303-402X
number of pages	14 (xsd:int)
http://bibframe.org/vocab/doi	10.1007/s00396-014-3236-6

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