About: Monodisperse macroporous poly(glycidyl methacrylate) microspheres coated with silica: Design, preparation and characterization     Goto   Sponge   NotDistinct   Permalink

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  • Monosized macroporous poly(glycidyl methacrylate) (PGMA) microspheres that were 9.3 μm in size were synthesized by multistep swelling polymerization using a modified Ugelstad technique. The PGMA microspheres and their hydrolyzed analogs derived from poly(2,3-dihydroxypropyl methacrylate) (PDHPMA) were coated by silanization with tetraethoxysilane (TEOS) and (3-aminopropyl)trimethoxysilane (APTES), respectively. The particles were characterized by elemental and thermogravimetric (TGA) analysis, scanning and transmission electron microscopy (SEM and TEM) coupled with an energy dispersive X-ray analysis (EDAX) and FT-IR spectroscopy to determine the SiO2 content, morphology, particle size, polydispersity and structure. These types of particles are expected to have improved biokompatibility relative to their starting polymers.
  • Monosized macroporous poly(glycidyl methacrylate) (PGMA) microspheres that were 9.3 μm in size were synthesized by multistep swelling polymerization using a modified Ugelstad technique. The PGMA microspheres and their hydrolyzed analogs derived from poly(2,3-dihydroxypropyl methacrylate) (PDHPMA) were coated by silanization with tetraethoxysilane (TEOS) and (3-aminopropyl)trimethoxysilane (APTES), respectively. The particles were characterized by elemental and thermogravimetric (TGA) analysis, scanning and transmission electron microscopy (SEM and TEM) coupled with an energy dispersive X-ray analysis (EDAX) and FT-IR spectroscopy to determine the SiO2 content, morphology, particle size, polydispersity and structure. These types of particles are expected to have improved biokompatibility relative to their starting polymers. (en)
Title
  • Monodisperse macroporous poly(glycidyl methacrylate) microspheres coated with silica: Design, preparation and characterization
  • Monodisperse macroporous poly(glycidyl methacrylate) microspheres coated with silica: Design, preparation and characterization (en)
skos:prefLabel
  • Monodisperse macroporous poly(glycidyl methacrylate) microspheres coated with silica: Design, preparation and characterization
  • Monodisperse macroporous poly(glycidyl methacrylate) microspheres coated with silica: Design, preparation and characterization (en)
skos:notation
  • RIV/61389013:_____/14:00425554!RIV14-MSM-61389013
http://linked.open...avai/riv/aktivita
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  • I, P(EE2.3.30.0029)
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  • April
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  • 30461
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  • RIV/61389013:_____/14:00425554
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  • multistep swelling polymerization; poly(glycidyl methacrylate); poly(2,3-dihydroxypropyl methacrylate) (en)
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  • NL - Nizozemsko
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  • [AC6FF3CE48CF]
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  • Reactive and Functional Polymers
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  • 77
http://linked.open...iv/tvurceVysledku
  • Horák, Daniel
  • Kovářová, Jana
  • Trchová, Miroslava
  • Beneš, Milan J.
  • Plichta, Zdeněk
  • Grama, Silvia
issn
  • 1381-5148
number of pages
http://bibframe.org/vocab/doi
  • 10.1016/j.reactfunctpolym.2014.01.010
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