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  • Pentafluoronitrosulfan, SF5NO2. (cs)
  • The synthesis of pentafluoronitrosulfane, SF5NO2, is accomplished either by reacting N(SF5)(3) with NO2 or by the photolysis of a SF5Br/NO2 mixture using diazo lamps. The product is purified by treatment with CsF and repeated trap-to-trap condensation. The solid compound melts at -78 degrees C, and the extrapolated boiling point is 9 degrees C. SF5NO2 is characterized by F-19, N-15 NMR, IR, Raman, and UV spectroscopy as well as by mass spectrometry. The molecular structure of SF5NO2 is determined by gas electron diffraction. The experimental geometry and vibrational spectrum are reproduced reasonably well by quantum chemical calculations.
  • The synthesis of pentafluoronitrosulfane, SF5NO2, is accomplished either by reacting N(SF5)(3) with NO2 or by the photolysis of a SF5Br/NO2 mixture using diazo lamps. The product is purified by treatment with CsF and repeated trap-to-trap condensation. The solid compound melts at -78 degrees C, and the extrapolated boiling point is 9 degrees C. SF5NO2 is characterized by F-19, N-15 NMR, IR, Raman, and UV spectroscopy as well as by mass spectrometry. The molecular structure of SF5NO2 is determined by gas electron diffraction. The experimental geometry and vibrational spectrum are reproduced reasonably well by quantum chemical calculations. (en)
Title
  • Pentafluoronitrosulfane, SF5NO2
  • Pentafluoronitrosulfan, SF5NO2 (cs)
  • Pentafluoronitrosulfane, SF5NO2 (en)
skos:prefLabel
  • Pentafluoronitrosulfane, SF5NO2
  • Pentafluoronitrosulfan, SF5NO2 (cs)
  • Pentafluoronitrosulfane, SF5NO2 (en)
skos:notation
  • RIV/61388980:_____/06:00040387!RIV07-AV0-61388980
http://linked.open.../vavai/riv/strany
  • 1783;1788
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(AV0Z40320502)
http://linked.open...iv/cisloPeriodika
  • 4
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 491729
http://linked.open...ai/riv/idVysledku
  • RIV/61388980:_____/06:00040387
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • electron-diffraction (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • US - Spojené státy americké
http://linked.open...ontrolniKodProRIV
  • [A4F9818F9A60]
http://linked.open...i/riv/nazevZdroje
  • Inorganic Chemistry
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 45
http://linked.open...iv/tvurceVysledku
  • Hnyk, Drahomír
  • Willner, H.
  • Oberhammer, H.
  • Lu, N.
  • Thrasher, J. S.
  • von Ahsen, S.
http://linked.open...n/vavai/riv/zamer
issn
  • 0020-1669
number of pages
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