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Description
| - Easily filtrated alumina-oxides spherical precursors were prepared by homogeneous precipitation from aluminium(III) sulphate with urea. Urea was employed as precipitation agent. X-Ray powder diffraction (XRD) spectra identified three different phases, namely: alpha-boehmite, boehmite and hydrobasaluminite. The morphology of prepared samples was observing by SEM (scanning electron microscopy) equipped with EDX (energy dispersive analysis by X-rays). The spherical clusters were examined at small concentration and the hydrobasaluminite islands were observed at the largest concentration of reagents. The microstructure characteristics were obtained by BET (Brunauer-Emmett-Teller) and BJH (Barrel-Joyner-Halanda) methods. BET in wide range from 6 to 142 m(2)/g and the all kinds of porous distribution were acquired, respectively. These methods showed that relationship between phase structures and microstructure exists.
- Easily filtrated alumina-oxides spherical precursors were prepared by homogeneous precipitation from aluminium(III) sulphate with urea. Urea was employed as precipitation agent. X-Ray powder diffraction (XRD) spectra identified three different phases, namely: alpha-boehmite, boehmite and hydrobasaluminite. The morphology of prepared samples was observing by SEM (scanning electron microscopy) equipped with EDX (energy dispersive analysis by X-rays). The spherical clusters were examined at small concentration and the hydrobasaluminite islands were observed at the largest concentration of reagents. The microstructure characteristics were obtained by BET (Brunauer-Emmett-Teller) and BJH (Barrel-Joyner-Halanda) methods. BET in wide range from 6 to 142 m(2)/g and the all kinds of porous distribution were acquired, respectively. These methods showed that relationship between phase structures and microstructure exists. (en)
- Snadno filtrovatelné sférické prekurzory oxidu hliníku byli připraveny homogenním srážením Al2(SO4)3 s močovinou ve vodném prostředí. Močovina se využívá jako precipitační činidlo. Produkt byl charakterizován práškovou rtg. difrakcí. Byly získané tři následující fáze: alfa-boehmite, boehmite and hydrobasaluminite. Morfologie byla pozorována pomocí skenovacího elektronového mikroskopu. Mikrostrukturní charakteristiky byly získány metodami BET a BJH. S rostoucím obsahem koncentrace reakčních látek se měnily nejenom fáze, ale také docházelo ke zvyšování iregularity morfologie. U alfa-boehmitu byly objeveny makropóry. V boehmitu byly objeveny mezopóry s makropóry a u hydrobasaluminitu byly všechny tři druhy pórů na stejné úrovni. (cs)
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Title
| - Hydrous aluminium-oxides prepared by homogeneous precipitation from aluminium(III)sulphate with urea
- Oxidy hlinité připravené homogenním srážením Al2(SO4)3 s močovinou ve vodném prostředí (cs)
- Hydrous aluminium-oxides prepared by homogeneous precipitation from aluminium(III)sulphate with urea (en)
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skos:prefLabel
| - Hydrous aluminium-oxides prepared by homogeneous precipitation from aluminium(III)sulphate with urea
- Oxidy hlinité připravené homogenním srážením Al2(SO4)3 s močovinou ve vodném prostředí (cs)
- Hydrous aluminium-oxides prepared by homogeneous precipitation from aluminium(III)sulphate with urea (en)
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skos:notation
| - RIV/61388980:_____/06:00040356!RIV07-MSM-61388980
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http://linked.open.../vavai/riv/strany
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http://linked.open...avai/riv/aktivita
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http://linked.open...avai/riv/aktivity
| - P(1M0577), Z(AV0Z40320502)
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http://linked.open...iv/cisloPeriodika
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http://linked.open...vai/riv/dodaniDat
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http://linked.open...aciTvurceVysledku
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http://linked.open.../riv/druhVysledku
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http://linked.open...iv/duvernostUdaju
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http://linked.open...titaPredkladatele
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http://linked.open...dnocenehoVysledku
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http://linked.open...ai/riv/idVysledku
| - RIV/61388980:_____/06:00040356
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http://linked.open...riv/jazykVysledku
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http://linked.open.../riv/klicovaSlova
| - urea; homogeneous precipitation; alpha-boehmite (en)
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http://linked.open.../riv/klicoveSlovo
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http://linked.open...odStatuVydavatele
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http://linked.open...ontrolniKodProRIV
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http://linked.open...i/riv/nazevZdroje
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http://linked.open...in/vavai/riv/obor
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http://linked.open...ichTvurcuVysledku
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http://linked.open...cetTvurcuVysledku
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http://linked.open...vavai/riv/projekt
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http://linked.open...UplatneniVysledku
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http://linked.open...v/svazekPeriodika
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http://linked.open...iv/tvurceVysledku
| - Szatmary, Lorant
- Šubrt, Jan
- Bakardjieva, Snejana
- Štengl, Václav
- Lukáč, Jozef
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http://linked.open...n/vavai/riv/zamer
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issn
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number of pages
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