About: N-Acylated Bacteriohopanehexol-Mannosamides from the Thermophilic Bacterium Alicyclobacillus acidoterrestris     Goto   Sponge   NotDistinct   Permalink

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  • Identification of molecular species of various N-acylated bacteriohopanehexol-mannosamides from the thermophilic bacterium Alicyclobacillus acidoterrestris by semipreparative HPLC and by RP-HPLC with ESI is described. We used triple-quadrupole type mass spectrometer, H-1 and C-13 NMR for analyzing this complex lipid. CD spectra of two compounds (model compound-7-deoxy-D-glycero-D-allo-heptitol obtained by stereospecific synthesis, and an isolated derivative of hopane) were also measured and the absolute configuration of both compounds was determined. On the basis of all the above methods, we identified the full structure of a new class of bacteriohopanes, represented by various N-acylated bacteriohopanehexol-mannosamides
  • Identification of molecular species of various N-acylated bacteriohopanehexol-mannosamides from the thermophilic bacterium Alicyclobacillus acidoterrestris by semipreparative HPLC and by RP-HPLC with ESI is described. We used triple-quadrupole type mass spectrometer, H-1 and C-13 NMR for analyzing this complex lipid. CD spectra of two compounds (model compound-7-deoxy-D-glycero-D-allo-heptitol obtained by stereospecific synthesis, and an isolated derivative of hopane) were also measured and the absolute configuration of both compounds was determined. On the basis of all the above methods, we identified the full structure of a new class of bacteriohopanes, represented by various N-acylated bacteriohopanehexol-mannosamides (en)
Title
  • N-Acylated Bacteriohopanehexol-Mannosamides from the Thermophilic Bacterium Alicyclobacillus acidoterrestris
  • N-Acylated Bacteriohopanehexol-Mannosamides from the Thermophilic Bacterium Alicyclobacillus acidoterrestris (en)
skos:prefLabel
  • N-Acylated Bacteriohopanehexol-Mannosamides from the Thermophilic Bacterium Alicyclobacillus acidoterrestris
  • N-Acylated Bacteriohopanehexol-Mannosamides from the Thermophilic Bacterium Alicyclobacillus acidoterrestris (en)
skos:notation
  • RIV/61388971:_____/11:00360792!RIV12-AV0-61388971
http://linked.open...avai/riv/aktivita
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  • P(1M06011), Z(AV0Z50200510)
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  • 3
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  • 214600
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  • RIV/61388971:_____/11:00360792
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  • Alicyclobacillus acidoterrestris; Negative RP-HPLC-ESI-MS/MS; Circular dichroism (en)
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  • US - Spojené státy americké
http://linked.open...ontrolniKodProRIV
  • [6F69CF5B3C71]
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  • Lipids
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  • 46
http://linked.open...iv/tvurceVysledku
  • Sigler, Karel
  • Siřišťová, L.
  • Řezanka, Tomáš
  • Melzoch, K.
http://linked.open...ain/vavai/riv/wos
  • 000288561500005
http://linked.open...n/vavai/riv/zamer
issn
  • 0024-4201
number of pages
http://bibframe.org/vocab/doi
  • 10.1007/s11745-010-3482-4
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