About: Analysis of insect triacylglycerols using liquid chromatography-atmospheric pressure chemical ionization-mass spectrometry     Goto   Sponge   NotDistinct   Permalink

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  • An HPLC non-aqueous reversed-phase separation system was adapted for analyzing insect triacylglycerols (TAG). The method uses two conventional Nova-Pak C18 columns connected in series, for a total length of 45 cm. The mobile phase gradient is mixed from acetonitrile and 2-propanol, and the flow rate is programmed from 1.0 to 0.7 mL/min. TAG are detected by atmospheric pressure chemical ionization mass spectrometry. The method ensures efficient separation of isomers and analysis of high-molecular weight TAG with equivalent chain lengths up to 72. The method performance is demonstrated on analysis of TAG isolated from the fat body of the bumblebee Bombus lucorum.
  • An HPLC non-aqueous reversed-phase separation system was adapted for analyzing insect triacylglycerols (TAG). The method uses two conventional Nova-Pak C18 columns connected in series, for a total length of 45 cm. The mobile phase gradient is mixed from acetonitrile and 2-propanol, and the flow rate is programmed from 1.0 to 0.7 mL/min. TAG are detected by atmospheric pressure chemical ionization mass spectrometry. The method ensures efficient separation of isomers and analysis of high-molecular weight TAG with equivalent chain lengths up to 72. The method performance is demonstrated on analysis of TAG isolated from the fat body of the bumblebee Bombus lucorum. (en)
Title
  • Analysis of insect triacylglycerols using liquid chromatography-atmospheric pressure chemical ionization-mass spectrometry
  • Analysis of insect triacylglycerols using liquid chromatography-atmospheric pressure chemical ionization-mass spectrometry (en)
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  • Analysis of insect triacylglycerols using liquid chromatography-atmospheric pressure chemical ionization-mass spectrometry
  • Analysis of insect triacylglycerols using liquid chromatography-atmospheric pressure chemical ionization-mass spectrometry (en)
skos:notation
  • RIV/61388963:_____/09:00326454!RIV10-MSM-61388963
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(2B06007), P(IAA4055403), S, Z(AV0Z40550506), Z(MSM6046137305)
http://linked.open...iv/cisloPeriodika
  • 5
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
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  • 302884
http://linked.open...ai/riv/idVysledku
  • RIV/61388963:_____/09:00326454
http://linked.open...riv/jazykVysledku
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  • atmospheric pressure chemical ionization; bumblebees; fat body; NARP-HPLC (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • DE - Spolková republika Německo
http://linked.open...ontrolniKodProRIV
  • [56F526BFEF46]
http://linked.open...i/riv/nazevZdroje
  • European Journal of Lipid Science and Technology
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
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http://linked.open...v/svazekPeriodika
  • 111
http://linked.open...iv/tvurceVysledku
  • Cvačka, Josef
  • Jiroš, Pavel
  • Kofroňová, Edita
  • Valterová, Irena
  • Sýkora, D.
http://linked.open...ain/vavai/riv/wos
  • 000266538000014
http://linked.open...n/vavai/riv/zamer
issn
  • 1438-7697
number of pages
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