About: Gas-Phase Mass-Transfer Characteristics of Mellapak 250Y Structured Packing under Distillation Conditions.     Goto   Sponge   NotDistinct   Permalink

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Description
  • The packing efficiency is usually presented in the form of the dependence of HETP on the load. As an integral quantity, HETP cannot be recalculated to another conditions, namely to other systems. This disadvantage is overcome when rate-based approach is applied instead, but the knowledge of the mass-transfer coefficients is inevitable. This contribution summarizes results of the measurement of the gas phase volumetric mass-transfer coefficient (kGa) for Mellapak 250Y structured packing under distillation conditions. The kGa has been determined using %22profile method%22 out of the molar fraction profiles along the column packing under the total reflux and atmospheric pressure for several alcohol systems and cyclohexane-heptane standard test system. The results demonstrate the agreement of kGa prediction of several dedicated mass-transfer models (Billet-Schultes, Rocha-Bravo-Fair, Delft model) with the experimental data. Revealed kGa dependence on the gas flow is also discussed. The different distribution of the mass-transfer resistance between the phases for alcohol and organic systems is demonstrated. Combination of the results with the extrapolation of the absorption derived ShG correlation enabled estimation of the distillation effective interfacial area, perhaps the most obscured mass-transfer parameter.
  • The packing efficiency is usually presented in the form of the dependence of HETP on the load. As an integral quantity, HETP cannot be recalculated to another conditions, namely to other systems. This disadvantage is overcome when rate-based approach is applied instead, but the knowledge of the mass-transfer coefficients is inevitable. This contribution summarizes results of the measurement of the gas phase volumetric mass-transfer coefficient (kGa) for Mellapak 250Y structured packing under distillation conditions. The kGa has been determined using %22profile method%22 out of the molar fraction profiles along the column packing under the total reflux and atmospheric pressure for several alcohol systems and cyclohexane-heptane standard test system. The results demonstrate the agreement of kGa prediction of several dedicated mass-transfer models (Billet-Schultes, Rocha-Bravo-Fair, Delft model) with the experimental data. Revealed kGa dependence on the gas flow is also discussed. The different distribution of the mass-transfer resistance between the phases for alcohol and organic systems is demonstrated. Combination of the results with the extrapolation of the absorption derived ShG correlation enabled estimation of the distillation effective interfacial area, perhaps the most obscured mass-transfer parameter. (en)
Title
  • Gas-Phase Mass-Transfer Characteristics of Mellapak 250Y Structured Packing under Distillation Conditions.
  • Gas-Phase Mass-Transfer Characteristics of Mellapak 250Y Structured Packing under Distillation Conditions. (en)
skos:prefLabel
  • Gas-Phase Mass-Transfer Characteristics of Mellapak 250Y Structured Packing under Distillation Conditions.
  • Gas-Phase Mass-Transfer Characteristics of Mellapak 250Y Structured Packing under Distillation Conditions. (en)
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  • RIV/60461373:22340/14:43897863!RIV15-GA0-22340___
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  • P(GA13-01251S), S
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  • 17938
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  • RIV/60461373:22340/14:43897863
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  • Mellapak; structured packing; mass-transfer; absorption (en)
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  • [1F4DB70F1123]
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  • New Orleans
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  • 14 AIChE Spring Meeting & 10th Global Congress on Process
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  • Rejl, František
  • Valenz, Lukáš
  • Haidl, Jan
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  • American Institute of Chemical Engineers
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  • 978-0-8169-1083-0
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  • 22340
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