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  • We developed slug-flow microfluidic systems for the enzyme hydrolysis of soybean oil. Because the enzyme, lipase, catalyzes various reactions at the water-oil interface, the use of well-defined slug flow microsystems can bring a promising alternative to classical systems. Two developed systems exploit biphasic oil-water slug flow formed in glass and teflon microcapillaries. The remaining system is able to generate stable three-phase slug flow nitrogen-(oil-water). Generation and characterization of the unique three-phase slug flow system are described in detail. It was found that the most stable oil-water slug flow can be realized by means of hydrophilic glass capillaries with the oil conversion about 30 % within 20 min. The highest triglyceride conversion (more than 40 % within 20 min) was attained in hydrophobic capillaries with instable two-phase slug flow. We identified the viscous stress to be the source of slug flow instabilities in the hydrophobic capillaries. The three-phase flow system produced regular segments of nitrogen separating small and regular oil-water emulsion compartments. In this system we obtained conversion about 35% within 20 min. We also mesured pressure drop in every type of microreactor.
  • We developed slug-flow microfluidic systems for the enzyme hydrolysis of soybean oil. Because the enzyme, lipase, catalyzes various reactions at the water-oil interface, the use of well-defined slug flow microsystems can bring a promising alternative to classical systems. Two developed systems exploit biphasic oil-water slug flow formed in glass and teflon microcapillaries. The remaining system is able to generate stable three-phase slug flow nitrogen-(oil-water). Generation and characterization of the unique three-phase slug flow system are described in detail. It was found that the most stable oil-water slug flow can be realized by means of hydrophilic glass capillaries with the oil conversion about 30 % within 20 min. The highest triglyceride conversion (more than 40 % within 20 min) was attained in hydrophobic capillaries with instable two-phase slug flow. We identified the viscous stress to be the source of slug flow instabilities in the hydrophobic capillaries. The three-phase flow system produced regular segments of nitrogen separating small and regular oil-water emulsion compartments. In this system we obtained conversion about 35% within 20 min. We also mesured pressure drop in every type of microreactor. (en)
Title
  • Microdevices for generation of two-phase and three-phase slug flows coupled with an enzyme reaction
  • Microdevices for generation of two-phase and three-phase slug flows coupled with an enzyme reaction (en)
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  • Microdevices for generation of two-phase and three-phase slug flows coupled with an enzyme reaction
  • Microdevices for generation of two-phase and three-phase slug flows coupled with an enzyme reaction (en)
skos:notation
  • RIV/60461373:22340/13:43895787!RIV14-MSM-22340___
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  • 88160
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  • RIV/60461373:22340/13:43895787
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  • frequency dependence; signal transmission; oscillatory flow; mathematical model (en)
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  • [78CBB0736224]
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  • Tatranské Matliare
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  • Bratislava
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  • Proceedings of the 40th International Conference of Slovak Society of Chemical Engineering
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  • Šnita, Dalimil
  • Přibyl, Michal
  • Čech, Jiří
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  • Slovak Society of Chemical Engineering
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  • 978-80-89475-09-4
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  • 22340
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