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  • The work deals with digital processing of experimental sorption data. The data in the course of vapour sorption during sorption experiment are distorted by random noise together with unwanted vibrations of the measurement scales. Before processing of data is necessary to remove the vibrations of the quartz scales caused by pressure surge after injection of a sample of vapour or gas. Elimination of the vibrations and correction of the data is carried out during their digital processing interactively by an experienced expert. Then the data are smoothed again interactively by application of the Savitzky-Golay filter. The parameters of sorption kinetics are determined from the corrected and smoothed sorption data automatically by means of the least squares method. The optimum value of the goal function is searched by multidimensional nonlinear optimization. Used Nelder-Mead method of flexible polyhedron requires only a mathematical model of sorption process, that is derived from the second Fick's law. The optimization process in addition to the value of diffusion coefficient calculates also the delay of the signal and its initial and steady-state values.
  • The work deals with digital processing of experimental sorption data. The data in the course of vapour sorption during sorption experiment are distorted by random noise together with unwanted vibrations of the measurement scales. Before processing of data is necessary to remove the vibrations of the quartz scales caused by pressure surge after injection of a sample of vapour or gas. Elimination of the vibrations and correction of the data is carried out during their digital processing interactively by an experienced expert. Then the data are smoothed again interactively by application of the Savitzky-Golay filter. The parameters of sorption kinetics are determined from the corrected and smoothed sorption data automatically by means of the least squares method. The optimum value of the goal function is searched by multidimensional nonlinear optimization. Used Nelder-Mead method of flexible polyhedron requires only a mathematical model of sorption process, that is derived from the second Fick's law. The optimization process in addition to the value of diffusion coefficient calculates also the delay of the signal and its initial and steady-state values. (en)
Title
  • Digital Processing of Noise Experimental Sorption Data using Savitzky-Golay filter
  • Digital Processing of Noise Experimental Sorption Data using Savitzky-Golay filter (en)
skos:prefLabel
  • Digital Processing of Noise Experimental Sorption Data using Savitzky-Golay filter
  • Digital Processing of Noise Experimental Sorption Data using Savitzky-Golay filter (en)
skos:notation
  • RIV/60461373:22340/13:43895098!RIV14-MSM-22340___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(MSM6046137306), Z(MSM6046137307)
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 69705
http://linked.open...ai/riv/idVysledku
  • RIV/60461373:22340/13:43895098
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • direct search optimization methods; Savitzky-Golay filter; digital signal processing; gravimetric sorption experiments (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...ontrolniKodProRIV
  • [58506B866CF9]
http://linked.open...v/mistoKonaniAkce
  • Tatranské Matliare
http://linked.open...i/riv/mistoVydani
  • Bratislava
http://linked.open...i/riv/nazevZdroje
  • Proceedings of the 40th International Conference of Slovak Society of Chemical Engineering
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...iv/tvurceVysledku
  • Friess, Karel
  • Hanta, Vladimír
  • Poživil, Jaroslav
http://linked.open...vavai/riv/typAkce
http://linked.open.../riv/zahajeniAkce
http://linked.open...n/vavai/riv/zamer
number of pages
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  • Slovak Society of Chemical Engineering
https://schema.org/isbn
  • 978-80-89475-09-4
http://localhost/t...ganizacniJednotka
  • 22340
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