About: Application of size exclusion chromatography - inductively coupled plasma - mass spectrometry for fractionation of element species in seeds of legumes

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	Fractionation of soluble species of P, Mn, Fe, Co, Ni, Cu, Zn, Se and Mo in pea and lentil seeds was made by on-line hyphenation of SEC and ICP-MS. Seed samples were extracted by 0.02 mol l-1 Tris-HCl buffer solution, pH=7.5. SEC was performed on Superdex 75 and Superdex Peptide columns (300 10 mm) with the same buffer solution as the mobile phase. Monitoring of oxide ion 47(PO)+ was used for detection of phosphorus compounds. Other elements were detected as ions of 55Mn, 57Fe, 59Co, 62Ni, 65Cu, 66Zn, 82Se and 95Mo nuclides. Elements in individual elution zones were quantified using external calibration. Complete chromatographic recoveries of elements were found in cases of phosphorus, nickel and copper. Substantial parts of manganese and zinc, as wellas traces of cobalt, selenium and molybdenum are retained on the column. Injection of EDTA solution removes these elements from the column. Chromatographic profiles of pea and lentil samples are very similar for all elements except Mo. Main element spec Fractionation of soluble species of P, Mn, Fe, Co, Ni, Cu, Zn, Se and Mo in pea and lentil seeds was made by on-line hyphenation of SEC and ICP-MS. Seed samples were extracted by 0.02 mol l-1 Tris-HCl buffer solution, pH=7.5. SEC was performed on Superdex 75 and Superdex Peptide columns (300 10 mm) with the same buffer solution as the mobile phase. Monitoring of oxide ion 47(PO)+ was used for detection of phosphorus compounds. Other elements were detected as ions of 55Mn, 57Fe, 59Co, 62Ni, 65Cu, 66Zn, 82Se and 95Mo nuclides. Elements in individual elution zones were quantified using external calibration. Complete chromatographic recoveries of elements were found in cases of phosphorus, nickel and copper. Substantial parts of manganese and zinc, as wellas traces of cobalt, selenium and molybdenum are retained on the column. Injection of EDTA solution removes these elements from the column. Chromatographic profiles of pea and lentil samples are very similar for all elements except Mo. Main element spec (en)
Title	Application of size exclusion chromatography - inductively coupled plasma - mass spectrometry for fractionation of element species in seeds of legumes Application of size exclusion chromatography - inductively coupled plasma - mass spectrometry for fractionation of element species in seeds of legumes (en)
skos:prefLabel	Application of size exclusion chromatography - inductively coupled plasma - mass spectrometry for fractionation of element species in seeds of legumes Application of size exclusion chromatography - inductively coupled plasma - mass spectrometry for fractionation of element species in seeds of legumes (en)
skos:notation	RIV/60461373:22340/02:00007174!RIV/2004/GA0/223404/N
http://linked.open.../vavai/riv/strany	179-187
http://linked.open...avai/riv/aktivita	P
http://linked.open...avai/riv/aktivity	P(GA525/00/0581)
http://linked.open...iv/cisloPeriodika	1
http://linked.open...vai/riv/dodaniDat	2004
http://linked.open...aciTvurceVysledku	Komínková, Jana Mestek, Oto Borková, Markéta Koplík, Richard Suchánek, Miloslav
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Vysoká škola chemicko-technologická v Praze / Fakulta chemicko-inženýrská
http://linked.open...dnocenehoVysledku	638834
http://linked.open...ai/riv/idVysledku	RIV/60461373:22340/02:00007174
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	Legumes; Size exclusion chromatography; Inductively coupled plasma mass spectrometry; phosphorus; trace elements (en)
http://linked.open.../riv/klicoveSlovo	Inductively coupled plasma mass spectrometry phosphorus Legumes trace elements Size exclusion chromatography
http://linked.open...odStatuVydavatele	NL - Nizozemsko
http://linked.open...ontrolniKodProRIV	[E64D6A772A90]
http://linked.open...i/riv/nazevZdroje	Journal of Chromatography B
http://linked.open...in/vavai/riv/obor	CB
http://linked.open...ichTvurcuVysledku	5 (xsd:int)
http://linked.open...cetTvurcuVysledku	5 (xsd:int)
http://linked.open...ocetUcastnikuAkce	0 (xsd:int)
http://linked.open...nichUcastnikuAkce	0 (xsd:int)
http://linked.open...vavai/riv/projekt	Speciation analysis of trace elements in foods
http://linked.open...UplatneniVysledku	2002
http://linked.open...v/svazekPeriodika	778
http://linked.open...iv/tvurceVysledku	Koplík, Richard Mestek, Oto Komínková, Jana Suchánek, Miloslav Borková, Markéta
issn	1570-0232
number of pages	9 (xsd:int)
http://localhost/t...ganizacniJednotka	22340

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