About: A fast and simple procedure for determination of perfluoroalkyl substances in food and feed: a method verification by an interlaboratory study

Facets (new session)
Description
Metadata
Settings
- owl:sameAs
- Inference Rule:

About: A fast and simple procedure for determination of perfluoroalkyl substances in food and feed: a method verification by an interlaboratory study Goto Sponge NotDistinct Permalink

An Entity of Type : http://linked.opendata.cz/ontology/domain/vavai/Vysledek, within Data Space : linked.opendata.cz associated with source document(s)

Attributes	Values
rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
rdfs:seeAlso	http://download.springer.com/static/pdf/132/art%253A10.1007%252Fs00216-013-6962-6.pdf?auth66=1393164636_85a5e4613323e9e7f69b47d92f2b286a&ext=.pdf
Description	In this study, a simple, fast, and cheap sample preparation procedure for the analysis of three well-known representatives of perfluoroalkyl substances (perfluorooctane sulfonate, perfluorooctanoic acid, and perfluorooctane sulfonamide) was validated in accordance with Commission Decision 2002/657/EC. The method was based on extraction with methanol followed by a dispersive solid phase extraction cleanup step by addition of activated charcoal for fish tissue, fish feed, and milk samples. The novel analytical approach combined with liquid chromatography?tandem mass spectrometry makes it possible to achieve limits of quantification below 1 ?g/kg (defined by Commission Recommendation 2010/161/EU). This method provides a high laboratory sample throughput: ten samples in 60 min. The validated procedure was successfully verified in an interlaboratory study. In this study, a simple, fast, and cheap sample preparation procedure for the analysis of three well-known representatives of perfluoroalkyl substances (perfluorooctane sulfonate, perfluorooctanoic acid, and perfluorooctane sulfonamide) was validated in accordance with Commission Decision 2002/657/EC. The method was based on extraction with methanol followed by a dispersive solid phase extraction cleanup step by addition of activated charcoal for fish tissue, fish feed, and milk samples. The novel analytical approach combined with liquid chromatography?tandem mass spectrometry makes it possible to achieve limits of quantification below 1 ?g/kg (defined by Commission Recommendation 2010/161/EU). This method provides a high laboratory sample throughput: ten samples in 60 min. The validated procedure was successfully verified in an interlaboratory study. (en)
Title	A fast and simple procedure for determination of perfluoroalkyl substances in food and feed: a method verification by an interlaboratory study A fast and simple procedure for determination of perfluoroalkyl substances in food and feed: a method verification by an interlaboratory study (en)
skos:prefLabel	A fast and simple procedure for determination of perfluoroalkyl substances in food and feed: a method verification by an interlaboratory study A fast and simple procedure for determination of perfluoroalkyl substances in food and feed: a method verification by an interlaboratory study (en)
skos:notation	RIV/60461373:22330/13:43896655!RIV14-MSM-22330___
http://linked.open...avai/riv/aktivita	P Z
http://linked.open...avai/riv/aktivity	P(7E08068), Z(MSM6046137305)
http://linked.open...iv/cisloPeriodika	24
http://linked.open...vai/riv/dodaniDat	2014
http://linked.open...aciTvurceVysledku	Hajšlová, Jana Pulkrabová, Jana Kocourek, Vladimír Hloušková, Veronika Hrádková, Petra Poustka, Jan
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Vysoká škola chemicko-technologická v Praze / Fakulta potravinářské a biochemické technologie
http://linked.open...dnocenehoVysledku	58604
http://linked.open...ai/riv/idVysledku	RIV/60461373:22330/13:43896655
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	, Commission Recommendation 2010/161/EU; Commission Decision 2002/657/E; method validation; liquid chromatography?tandem mass spectrometry; activated charcoal; Perfluoroalkyl substances (en)
http://linked.open.../riv/klicoveSlovo	Commission Decision 2002/657/E Commission Recommendation 2010/161/EU Perfluoroalkyl substances activated charcoal liquid chromatography?tandem mass spectrometry method validation
http://linked.open...odStatuVydavatele	DE - Spolková republika Německo
http://linked.open...ontrolniKodProRIV	[1C99DDCDC317]
http://linked.open...i/riv/nazevZdroje	Analytical and Bioanalytical Chemistry
http://linked.open...in/vavai/riv/obor	GM
http://linked.open...ichTvurcuVysledku	6 (xsd:int)
http://linked.open...cetTvurcuVysledku	9 (xsd:int)
http://linked.open...vavai/riv/projekt	CONtaminants in Food and Feed: Inexpensive DEtectioN for Control of Exposure
http://linked.open...UplatneniVysledku	2013
http://linked.open...v/svazekPeriodika	405
http://linked.open...iv/tvurceVysledku	Hajšlová, Jana Pulkrabová, Jana Kocourek, Vladimír Hrádková, Petra Poustka, Jan Barceló, D. Farré, M. Llorca, M. Švihlíková, Veronika
http://linked.open...ain/vavai/riv/wos	000324109400023
http://linked.open...n/vavai/riv/zamer	Teoretické základy potravinářských a biochemických technologií
issn	1618-2642
number of pages	11 (xsd:int)
http://bibframe.org/vocab/doi	10.1007/s00216-013-6962-6
http://localhost/t...ganizacniJednotka	22330

Faceted Search & Find service v1.16.118 as of Jun 21 2024

Alternative Linked Data Documents: ODE Content Formats:

RDF

ODATA

Microdata

About

OpenLink Virtuoso version 07.20.3240 as of Jun 21 2024, on Linux (x86_64-pc-linux-gnu), Single-Server Edition (126 GB total memory, 41 GB memory in use)
Data on this page belongs to its respective rights holders.
Virtuoso Faceted Browser Copyright © 2009-2024 OpenLink Software