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rdf:type
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Description
| - The objective of the presented study was to develop and optimize a simple, high-throughput method for the control of 32 mycotoxins (Fusarium and Alternaria toxins, aflatoxins, ergot alkaloids, ochratoxins, and sterigmatocystin) in beer. Due to the broad range of their physicochemical properties, the sample preparation step was simplified as much as possible to avoid analyte losses. The addition of acetonitrile to beer samples enabled precipitation of abundant matrix components. The clean-up efficiency was controlled by ambientmass spectrometry employing a direct analysis in real time (DART) ion source. For determination of analytes, ultra-high-performance liquid chromatogramy hyphenated with high-resolution mass spectrometry utilizing an orbitrap (U-HPLC?orbitrapMS) or time-of-flight (TOFMS) technology was used. Because of significantly better detection capabilities of the orbitrap technology, the U-HPLC?orbitrapMSmethod was chosen as a determinative step and fully validated. To compensate matrix
- The objective of the presented study was to develop and optimize a simple, high-throughput method for the control of 32 mycotoxins (Fusarium and Alternaria toxins, aflatoxins, ergot alkaloids, ochratoxins, and sterigmatocystin) in beer. Due to the broad range of their physicochemical properties, the sample preparation step was simplified as much as possible to avoid analyte losses. The addition of acetonitrile to beer samples enabled precipitation of abundant matrix components. The clean-up efficiency was controlled by ambientmass spectrometry employing a direct analysis in real time (DART) ion source. For determination of analytes, ultra-high-performance liquid chromatogramy hyphenated with high-resolution mass spectrometry utilizing an orbitrap (U-HPLC?orbitrapMS) or time-of-flight (TOFMS) technology was used. Because of significantly better detection capabilities of the orbitrap technology, the U-HPLC?orbitrapMSmethod was chosen as a determinative step and fully validated. To compensate matrix (en)
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Title
| - Analysis of multiple mycotoxins in beer employing (ultra)-high resolution mass spectrometry.
- Analysis of multiple mycotoxins in beer employing (ultra)-high resolution mass spectrometry. (en)
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skos:prefLabel
| - Analysis of multiple mycotoxins in beer employing (ultra)-high resolution mass spectrometry.
- Analysis of multiple mycotoxins in beer employing (ultra)-high resolution mass spectrometry. (en)
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skos:notation
| - RIV/60461373:22330/10:00024320!RIV11-MSM-22330___
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http://linked.open...avai/riv/aktivita
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http://linked.open...avai/riv/aktivity
| - P(1M0570), P(2B08049), R, Z(MSM6046137305)
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http://linked.open...iv/cisloPeriodika
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http://linked.open...vai/riv/dodaniDat
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http://linked.open...aciTvurceVysledku
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http://linked.open.../riv/druhVysledku
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http://linked.open...iv/duvernostUdaju
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http://linked.open...titaPredkladatele
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http://linked.open...dnocenehoVysledku
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http://linked.open...ai/riv/idVysledku
| - RIV/60461373:22330/10:00024320
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http://linked.open...riv/jazykVysledku
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http://linked.open.../riv/klicovaSlova
| - mycotoxins; beer; high resolution mass spectrometry (en)
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http://linked.open.../riv/klicoveSlovo
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http://linked.open...odStatuVydavatele
| - GB - Spojené království Velké Británie a Severního Irska
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http://linked.open...ontrolniKodProRIV
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http://linked.open...i/riv/nazevZdroje
| - Rapid Communications in Mass Spectrometry
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http://linked.open...in/vavai/riv/obor
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http://linked.open...ichTvurcuVysledku
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http://linked.open...cetTvurcuVysledku
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http://linked.open...vavai/riv/projekt
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http://linked.open...UplatneniVysledku
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http://linked.open...v/svazekPeriodika
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http://linked.open...iv/tvurceVysledku
| - Hajšlová, Jana
- Zachariášová, Milena
- Čajka, Tomáš
- Godula, Michal
- Vepříková, Zdenka
- Krplová, Alexandra
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http://linked.open...ain/vavai/riv/wos
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http://linked.open...n/vavai/riv/zamer
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issn
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number of pages
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http://localhost/t...ganizacniJednotka
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