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Description
  • A capillary zone electrophoresis (CZE) method with conductometric detection of biogenic amines (cadaverine, putrescine, agmatine, histamine, tryptamine and tyramine) is described. The optimised background electrolyte was following: 15 mM histidine + 5 mM adipic acid + 1.5 mM sulphuric acid + 0.1 mM ethylenediaminotetraacetic acid + 0.1% hydroxyethylcellulose + 50% methanol. A clear separation of six biogenic amines from other components of acidic sample extract was achieved within 10 min. Method characteristics, i.e., linearity (0 - 100 nmol/ml), accuracy (recovery 86 - 107 %), intra-assay repeatability (2 - 4 %), and detection limit (2-5 nmol/ml) were evaluated. Low laboriousness, sufficient sensitivity, speed of analysis, and low running cost are important attributes of this method. The developed method was successfully applied on the determination of biogenic amines in selected food samples.
  • A capillary zone electrophoresis (CZE) method with conductometric detection of biogenic amines (cadaverine, putrescine, agmatine, histamine, tryptamine and tyramine) is described. The optimised background electrolyte was following: 15 mM histidine + 5 mM adipic acid + 1.5 mM sulphuric acid + 0.1 mM ethylenediaminotetraacetic acid + 0.1% hydroxyethylcellulose + 50% methanol. A clear separation of six biogenic amines from other components of acidic sample extract was achieved within 10 min. Method characteristics, i.e., linearity (0 - 100 nmol/ml), accuracy (recovery 86 - 107 %), intra-assay repeatability (2 - 4 %), and detection limit (2-5 nmol/ml) were evaluated. Low laboriousness, sufficient sensitivity, speed of analysis, and low running cost are important attributes of this method. The developed method was successfully applied on the determination of biogenic amines in selected food samples. (en)
  • A capillary zone electrophoresis (CZE) method with conductometric detection of biogenic amines (cadaverine, putrescine, agmatine, histamine, tryptamine and tyramine) is described. The optimised background electrolyte was following: 15 mM histidine + 5 mM adipic acid + 1.5 mM sulphuric acid + 0.1 mM ethylenediaminotetraacetic acid + 0.1% hydroxyethylcellulose + 50% methanol. A clear separation of six biogenic amines from other components of acidic sample extract was achieved within 10 min. Method characteristics, i.e., linearity (0 - 100 nmol/ml), accuracy (recovery 86 - 107 %), intra-assay repeatability (2 - 4 %), and detection limit (2-5 nmol/ml) were evaluated. Low laboriousness, sufficient sensitivity, speed of analysis, and low running cost are important attributes of this method. The developed method was successfully applied on the determination of biogenic amines in selected food samples. (cs)
Title
  • Determination of biogenic amines by capillary zone electrophoresis with conductometric detection
  • Determination of biogenic amines by capillary zone electrophoresis with conductometric detection (en)
  • Stanovení biogenních aminů kapilární zónovou elektroforesou s vodivostní detekcí (cs)
skos:prefLabel
  • Determination of biogenic amines by capillary zone electrophoresis with conductometric detection
  • Determination of biogenic amines by capillary zone electrophoresis with conductometric detection (en)
  • Stanovení biogenních aminů kapilární zónovou elektroforesou s vodivostní detekcí (cs)
skos:notation
  • RIV/60461373:22330/06:00016406!RIV07-MSM-22330___
http://linked.open.../vavai/riv/strany
  • 145-149
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(GA525/03/0351), Z(MSM6046137305)
http://linked.open...iv/cisloPeriodika
  • 1103
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 471114
http://linked.open...ai/riv/idVysledku
  • RIV/60461373:22330/06:00016406
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • Biogenic amines; capillary zone electrophoresis; food; conductivity detection (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • NL - Nizozemsko
http://linked.open...ontrolniKodProRIV
  • [F18FF0EF8D55]
http://linked.open...i/riv/nazevZdroje
  • Journal of Chromatography A
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...iv/tvurceVysledku
  • Voldřich, Michal
  • Kvasnička, František
http://linked.open...n/vavai/riv/zamer
issn
  • 0021-9673
number of pages
http://localhost/t...ganizacniJednotka
  • 22330
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