About: COMPARISON CONVENTIONAL HPLC/MS WITH UP-TODAY UPLC/MS METHOD FOR ANALYSIS OF 67 POLAR PESTICIDES

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	The up-today UPLC (Ultra Performance Liquid Chromatography) Acquity systém serves a lot of advantages in the area of polar pesticide analysis. The Waters Acquity system works at high pressures (up to 15.000 psi) with BEH columns. Thanks to these chromatographic parameters, providing high resolution that allows faster separation. For determination of 67 polar pesticides it is commonly used HPLC/MS Waters Aliance 2695 / Quattro Premier. This analytical method is accredited (ISO 17025) and detections limits (LOD) of all analytes are under the hygienic limits for baby food (MRL=0.010 mg/kg). For separation Supelco Discovery C-18 (150 mm, 3 mm, 5 mm) was used with mobile phase gradient of 0.01M ammonium acetate in water/MetOH and flow rate 0.3 ml/min. The analysis is finished in 50 min, so within 24 hours 16 samples can by analyzed including calibration curves and QC samples. This method was transferred and optimized on Waters UPLC Acquity system coupled with Waters Quattro Premier. For separation BEH C-18 The up-today UPLC (Ultra Performance Liquid Chromatography) Acquity systém serves a lot of advantages in the area of polar pesticide analysis. The Waters Acquity system works at high pressures (up to 15.000 psi) with BEH columns. Thanks to these chromatographic parameters, providing high resolution that allows faster separation. For determination of 67 polar pesticides it is commonly used HPLC/MS Waters Aliance 2695 / Quattro Premier. This analytical method is accredited (ISO 17025) and detections limits (LOD) of all analytes are under the hygienic limits for baby food (MRL=0.010 mg/kg). For separation Supelco Discovery C-18 (150 mm, 3 mm, 5 mm) was used with mobile phase gradient of 0.01M ammonium acetate in water/MetOH and flow rate 0.3 ml/min. The analysis is finished in 50 min, so within 24 hours 16 samples can by analyzed including calibration curves and QC samples. This method was transferred and optimized on Waters UPLC Acquity system coupled with Waters Quattro Premier. For separation BEH C-18 (en) Porovnání konvenční HPLC/MS s moderní UPLC/MS v analýze 67 polárních pesticidů (cs)
Title	COMPARISON CONVENTIONAL HPLC/MS WITH UP-TODAY UPLC/MS METHOD FOR ANALYSIS OF 67 POLAR PESTICIDES COMPARISON CONVENTIONAL HPLC/MS WITH UP-TODAY UPLC/MS METHOD FOR ANALYSIS OF 67 POLAR PESTICIDES (en) Porovnání konvenční HPLC/MS s moderní UPLC/MS v analýze 67 polárních pesticidů (cs)
skos:prefLabel	COMPARISON CONVENTIONAL HPLC/MS WITH UP-TODAY UPLC/MS METHOD FOR ANALYSIS OF 67 POLAR PESTICIDES COMPARISON CONVENTIONAL HPLC/MS WITH UP-TODAY UPLC/MS METHOD FOR ANALYSIS OF 67 POLAR PESTICIDES (en) Porovnání konvenční HPLC/MS s moderní UPLC/MS v analýze 67 polárních pesticidů (cs)
skos:notation	RIV/60461373:22330/05:00015505!RIV06-MSM-22330___
http://linked.open...avai/riv/aktivita	Z
http://linked.open...avai/riv/aktivity	Z(MSM 223300004)
http://linked.open...vai/riv/dodaniDat	2006
http://linked.open...aciTvurceVysledku	Hajšlová, Jana Poustka, Jan Kovalczuk, Tomáš
http://linked.open.../riv/druhVysledku	O - Ostatní výsledky nezařaditelné do žádného z výše uvedených druhů výsledku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Vysoká škola chemicko-technologická v Praze / Fakulta potravinářské a biochemické technologie
http://linked.open...dnocenehoVysledku	515816
http://linked.open...ai/riv/idVysledku	RIV/60461373:22330/05:00015505
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	HPLC/MS; UPLC/MS; analýza; polární pesticidy (en)
http://linked.open.../riv/klicoveSlovo	HPLC/MS UPLC/MS analýza polární pesticidy
http://linked.open...ontrolniKodProRIV	[9D871E0E4B15]
http://linked.open...in/vavai/riv/obor	GM
http://linked.open...ichTvurcuVysledku	3 (xsd:int)
http://linked.open...cetTvurcuVysledku	4 (xsd:int)
http://linked.open...UplatneniVysledku	2005
http://linked.open...iv/tvurceVysledku	Hajšlová, Jana Kovalczuk, Tomáš Poustka, Jan Jech, Martin
http://linked.open...n/vavai/riv/zamer	http://linked.opendata.cz/resource/domain/vavai/zamer/MSM%20223300004
http://localhost/t...ganizacniJednotka	22330

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