About: Potential of Liquid Chromatography - Atmospheric Pressure Chemical Ionisation Tandem Mass Spectrometry for Determination of Fosetyl-aluminium Residues in Dried Hops

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	New analytical procedure for the determination of fosetyl-aluminium in hop cones (also called %22hops%22) was developed. Liquid chromatography-atmospheric pressure chemical ionisation tandem mass spectrometry (LC-APCIMS/MS) allowed a highly selective determination of this fungicide which facilitated the sample preparation. The sufficiently low detection limit (1 mg/kg of dried hops) with the acceptable method performance characteristics (RSD 9%, recovery 76% - at the level of 10 mg/kg) complies with the need to inspect the observance of maximal residual limit 100 mg/kg. The application of LC-MS technique thus provided an effective way of fosetyl-aluminium determination in the complex hops matrix. New analytical procedure for the determination of fosetyl-aluminium in hop cones (also called %22hops%22) was developed. Liquid chromatography-atmospheric pressure chemical ionisation tandem mass spectrometry (LC-APCIMS/MS) allowed a highly selective determination of this fungicide which facilitated the sample preparation. The sufficiently low detection limit (1 mg/kg of dried hops) with the acceptable method performance characteristics (RSD 9%, recovery 76% - at the level of 10 mg/kg) complies with the need to inspect the observance of maximal residual limit 100 mg/kg. The application of LC-MS technique thus provided an effective way of fosetyl-aluminium determination in the complex hops matrix. (en) Možnosti kapalinové chromatografie-tandemové hmotnostní spektrometrie s chemickou ionizací za atmosférického tlaku při stanovení reziduí fosetyl-aluminia v sušených chmelových šišticích (cs)
Title	Možnosti kapalinové chromatografie-tandemové hmotnostní spektrometrie s chemickou ionizací za atmosférického tlaku při stanovení reziduí fosetyl-aluminia v sušených chmelových šišticích (cs) Potential of Liquid Chromatography - Atmospheric Pressure Chemical Ionisation Tandem Mass Spectrometry for Determination of Fosetyl-aluminium Residues in Dried Hops Potential of Liquid Chromatography - Atmospheric Pressure Chemical Ionisation Tandem Mass Spectrometry for Determination of Fosetyl-aluminium Residues in Dried Hops (en)
skos:prefLabel	Možnosti kapalinové chromatografie-tandemové hmotnostní spektrometrie s chemickou ionizací za atmosférického tlaku při stanovení reziduí fosetyl-aluminia v sušených chmelových šišticích (cs) Potential of Liquid Chromatography - Atmospheric Pressure Chemical Ionisation Tandem Mass Spectrometry for Determination of Fosetyl-aluminium Residues in Dried Hops Potential of Liquid Chromatography - Atmospheric Pressure Chemical Ionisation Tandem Mass Spectrometry for Determination of Fosetyl-aluminium Residues in Dried Hops (en)
skos:notation	RIV/60461373:22330/04:00013122!RIV/2005/MSM/223305/N
http://linked.open.../vavai/riv/strany	24-28
http://linked.open...avai/riv/aktivita	Z
http://linked.open...avai/riv/aktivity	Z(MSM 223300004)
http://linked.open...iv/cisloPeriodika	1
http://linked.open...vai/riv/dodaniDat	2005
http://linked.open...aciTvurceVysledku	Riddellová, Kateřina Hajšlová, Jana Poustka, Jan
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Vysoká škola chemicko-technologická v Praze / Fakulta potravinářské a biochemické technologie
http://linked.open...dnocenehoVysledku	580763
http://linked.open...ai/riv/idVysledku	RIV/60461373:22330/04:00013122
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	fosetyl-aluminium;pesticide residues;hops analysis;liquid chromatography;mass spectrometry (en)
http://linked.open.../riv/klicoveSlovo	fosetyl-aluminium hops analysis pesticide residues liquid chromatography mass spectrometry
http://linked.open...odStatuVydavatele	CZ - Česká republika
http://linked.open...ontrolniKodProRIV	[46E68A7AF483]
http://linked.open...i/riv/nazevZdroje	Czech Journal of Food Science
http://linked.open...in/vavai/riv/obor	GM
http://linked.open...ichTvurcuVysledku	3 (xsd:int)
http://linked.open...cetTvurcuVysledku	4 (xsd:int)
http://linked.open...UplatneniVysledku	2004
http://linked.open...v/svazekPeriodika	22
http://linked.open...iv/tvurceVysledku	Hajšlová, Jana Nováková, K. Poustka, Jan Holadová, Kateřina
http://linked.open...n/vavai/riv/zamer	http://linked.opendata.cz/resource/domain/vavai/zamer/MSM%20223300004
issn	1212-1800
number of pages	5 (xsd:int)
http://localhost/t...ganizacniJednotka	22330

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