About: Determination of vinyl chloride monomer in food contact materials by solid phase microextraction coupled with gas chromatography/mass spectrometry     Goto   Sponge   NotDistinct   Permalink

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  • The present study concerns the optimisation of the headspace solid phase microextraction (HS/SPME) combined with gas chromatography/mass spectrometry (GC/MS) for the vinyl chloride monomer determination. Samples of PVC materials were analysed using the Carboxen/Polydimethylsiloxane (CX/PDMS) 75 #m fibre. For this fibre, the achieved limit of detection was 0.05 #g/kg, and that of quantification 0.17 #g/kg, respectively, with RSD 5%. The levels of VCM found ranged from 0.29 to 0.44 mg/kg, in the case of foil, the VCM content determined was 3.65 mg/kg which means that the maximal limit allowed was exceeded.
  • The present study concerns the optimisation of the headspace solid phase microextraction (HS/SPME) combined with gas chromatography/mass spectrometry (GC/MS) for the vinyl chloride monomer determination. Samples of PVC materials were analysed using the Carboxen/Polydimethylsiloxane (CX/PDMS) 75 #m fibre. For this fibre, the achieved limit of detection was 0.05 #g/kg, and that of quantification 0.17 #g/kg, respectively, with RSD 5%. The levels of VCM found ranged from 0.29 to 0.44 mg/kg, in the case of foil, the VCM content determined was 3.65 mg/kg which means that the maximal limit allowed was exceeded. (en)
Title
  • Determination of vinyl chloride monomer in food contact materials by solid phase microextraction coupled with gas chromatography/mass spectrometry
  • Determination of vinyl chloride monomer in food contact materials by solid phase microextraction coupled with gas chromatography/mass spectrometry (en)
skos:prefLabel
  • Determination of vinyl chloride monomer in food contact materials by solid phase microextraction coupled with gas chromatography/mass spectrometry
  • Determination of vinyl chloride monomer in food contact materials by solid phase microextraction coupled with gas chromatography/mass spectrometry (en)
skos:notation
  • RIV/60461373:22330/03:00008845!RIV/2004/MSM/223304/N
http://linked.open.../vavai/riv/strany
  • 13-17
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(MSM 223300004)
http://linked.open...iv/cisloPeriodika
  • 1
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 603411
http://linked.open...ai/riv/idVysledku
  • RIV/60461373:22330/03:00008845
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • migration, solid phase microextraction (SPME), vinyl chloride monomer (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • CZ - Česká republika
http://linked.open...ontrolniKodProRIV
  • [207C262432E4]
http://linked.open...i/riv/nazevZdroje
  • Czech Journal of Food Science
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...ocetUcastnikuAkce
http://linked.open...nichUcastnikuAkce
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 21
http://linked.open...iv/tvurceVysledku
  • Dobiáš, Jaroslav
  • Voldřich, Michal
  • Poustka, Jan
  • Jordáková, Ivana
http://linked.open...n/vavai/riv/zamer
issn
  • 1212-1800
number of pages
http://localhost/t...ganizacniJednotka
  • 22330
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